Search results for " Size"
showing 10 items of 2281 documents
X-ray diffraction line broadening on vibrating dry-milled Two Crows sepiolite
2006
A reference sample of sepiolite and products of its comminution by vibrating dry-milling have been studied using X-ray diffraction (XRD) line-broadening analysis, complementary field emission scanning electron microscopy (FESEM) images and surface area measurements. The apparent crystallite sizes determined via XRD are in agreement with observations on FESEM images. The sepiolite aggregates consist of lath-shaped agglutinations of prisms and pinacoids elongated along [001], each lath including several crystallites in that direction. The surface area magnitudes are in the range of previous experimental measurements of other sepiolites. The results obtained show the effectiveness of vibro-mil…
Analysis of Dissolved-Gas Atomization: Supercritical CO2 Dissolved in Water
2010
Supercritical dissolved-gas atomization is an atomization process in which carbon dioxide at temperature and pressure above its critical point is used as the atomizing gas. The spray characteristics in terms of droplets size and distribution have been experimentally studied using a laser diffraction method based on a Malvern apparatus. The main parameter that influences the droplets size is the gas-to-liquid mass ratio (GLR); the injection pressure in the range of 7.4-13 MPa has a minor effect. Upon variation of the GLR from 0.5 to 3, the droplet mean diameter changes from about 8.0 to 2.0 μm; very narrow droplet size distributions are also produced. From the point of view of the atomizatio…
A multi-step mechanism and integrity of titanate nanoribbons.
2014
A one-step hydrothermal treatment of TiO2 powders under strongly basic conditions has been used to synthesize titanate nanoribbons. The nanoparticles were thoroughly characterized using several methods including transmission electron microscopy (TEM), X-ray diffraction (XRD), Raman spectroscopy and X-ray photoelectron spectrometry (XPS) to determine their morphological, structural and chemical characteristics. The influence of the nature and size of the TiO2 precursor and of the reaction duration on the formation of the nanoribbons was investigated. The conditions required to obtain only titanate nanoribbons with a width ranging from 100 to 200 nm and several tens of micrometers in length w…
Assessing the particle size of a broadly dispersed powder by complementary techniques
1998
The experimental determination of reliable particle size distribution curves and statistical parameters of broad distributions is known to be a difficult task. This problem is addressed here in an attempt to characterize the granularity of three distinct batches of a pharmaceutical powder (fenofibrate from Fournier Laboratories). The methodology consists in comparing the results, expressed in terms of surface based mean diameter, as obtained by three complementary techniques, namely optical microscopy image analysis, laser light low angle diffraction and surface area measurement by krypton physisorption. These techniques are applied in parallel to the material of interest and to a certified…
Inorganic gels as precursors of TiO2 photocatalysts prepared by low temperature microwave or thermal treatment
2008
Abstract A simple procedure for preparing active TiO2 photocatalysts is presented. The starting materials were unusual TiO2 gels formed from TiCl4. The use of microwaves for a very short time enhanced the TiO2 crystallinity preventing an increase of particle size and minimizing the decrease of specific surface area. This result makes this preparation very attractive. The formation of the gels was monitored through measurements of viscosity. All the samples were characterized by means of X-ray diffraction, diffuse reflectance spectroscopy and BET specific surface area measurements. The photoactivity of the samples was evaluated using the photodegradation of 4-nitrophenol in liquid–solid regi…
RADIUS - rapid particle analysis of digital images by ultra-high-resolution scanning of thin sections
2005
RADIUS is a newly developed particle-size measurement technique, based on evaluation of digital images of thin sections. Analyses are performed with sub-millimetre sample resolution and are thus designed to work on a single lamina of laminated sediments. The method covers grain sizes from medium silt to coarse sand. The application contains pattern-recognition modules that allow the detection of typical particle distributions of loess, organic detritus, turbidites and tephra layers. Cutting and hiding effects of particles on thin sections are corrected by empirical correction matrices. The calculated analysis results are compared with manually counted and measured samples to calibrate the a…
Optimal Population Growth as an Endogenous Discounting Problem: The Ramsey Case
2018
International audience; This paper revisits the optimal population size problem in a continuous time Ramsey setting with costly child rearing and both intergenerational and intertemporal altruism. The social welfare functions considered range from the Millian to the Benthamite. When population growth is endogenized, the associated optimal control problem involves an endogenous effective discount rate depending on past and current population growth rates, which makes preferences intertemporally dependent. We tackle this problem by using an appropriate maximum principle. Then we study the stationary solutions (balanced growth paths) and show the existence of two admissible solutions except in…
The minimum size of fully irregular oriented graphs
2001
Abstract Digraphs in which any two vertices have different pairs of semi-degrees are called fully irregular. For n-vertex fully irregular oriented graphs (i.e. digraphs without loops or 2-dicycles) the minimum size is presented.
Parsimony hierarchies for inductive inference
2004
AbstractFreivalds defined an acceptable programming system independent criterion for learning programs for functions in which the final programs were required to be both correct and “nearly” minimal size. i.e.. within a computable function of being purely minimal size. Kinber showed that this parsimony requirement on final programs limits learning power. However, in scientific inference, parsimony is considered highly desirable. Alim-computable functionis (by definition) one calculable by a total procedure allowed to change its mind finitely many times about its output. Investigated is the possibility of assuaging somewhat the limitation on learning power resulting from requiring parsimonio…
Groups whose prime graph on conjugacy class sizes has few complete vertices
2012
Abstract Let G be a finite group, and let Γ ( G ) denote the prime graph built on the set of conjugacy class sizes of G. In this paper, we consider the situation when Γ ( G ) has “few complete vertices”, and our aim is to investigate the influence of this property on the group structure of G. More precisely, assuming that there exists at most one vertex of Γ ( G ) that is adjacent to all the other vertices, we show that G is solvable with Fitting height at most 3 (the bound being the best possible). Moreover, if Γ ( G ) has no complete vertices, then G is a semidirect product of two abelian groups having coprime orders. Finally, we completely characterize the case when Γ ( G ) is a regular …