Search results for "acids"

showing 10 items of 3520 documents

Expression in Escherichia coli of Native and Chimeric Phenolic Acid Decarboxylases with Modified Enzymatic Activities and Method for Screening Recomb…

2001

ABSTRACT Four bacterial phenolic acid decarboxylases (PAD) from Lactobacillus plantarum , Pediococcus pentosaceus , Bacillus subtilis , and Bacillus pumilus were expressed in Escherichia coli , and their activities on p -coumaric, ferulic, and caffeic acids were compared. Although these four enzymes displayed 61% amino acid sequence identity, they exhibit different activities for ferulic and caffeic acid metabolism. To elucidate the domain(s) that determines these differences, chimeric PAD proteins were constructed and expressed in E. coli by exchanging their individual carboxy-terminal portions. Analysis of the chimeric enzyme activities suggests that the C-terminal region may be involved …

Carboxy-lyasesCoumaric AcidsCarboxy-LyasesDecarboxylationRecombinant Fusion ProteinsBacillus subtilismedicine.disease_causeApplied Microbiology and BiotechnologySubstrate Specificitychemistry.chemical_compoundCaffeic AcidsEscherichia coliCaffeic acidmedicineAmino Acid SequenceEnzymology and Protein EngineeringEscherichia colichemistry.chemical_classificationBacteriaEcologybiologyBacillus pumilusSequence Analysis DNAPhenolic acidbiology.organism_classificationCulture MediaEnzymechemistryBiochemistryFood ScienceBiotechnologyApplied and Environmental Microbiology
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Knockout of thep-Coumarate Decarboxylase Gene fromLactobacillus plantarumReveals the Existence of Two Other Inducible Enzymatic Activities Involved i…

2000

ABSTRACTLactobacillus plantarumNC8 contains apdcgene coding forp-coumaric acid decarboxylase activity (PDC). A food grade mutant, designated LPD1, in which the chromosomalpdcgene was replaced with the deletedpdcgene copy, was obtained by a two-step homologous recombination process using an unstable replicative vector. The LPD1 mutant strain remained able to weakly metabolizep-coumaric and ferulic acids into vinyl derivatives or into substituted phenyl propionic acids. We have shown thatL. plantarumhas a second acid phenol decarboxylase enzyme, better induced with ferulic acid than withp-coumaric acid, which also displays inducible acid phenol reductase activity that is mostly active when gl…

Carboxy-lyasesCoumaric AcidsCarboxy-LyasesMutantGenetics and Molecular Biologymacromolecular substancesCoumaric acidApplied Microbiology and BiotechnologyFerulic acidchemistry.chemical_compoundHydroxybenzoatesCloning Molecularchemistry.chemical_classificationEcologybiologyhemic and immune systemsMetabolismPhenolic acidHydrogen-Ion Concentrationbiology.organism_classificationLactobacillusElectroporationEnzymechemistryBiochemistryEnzyme InductionPropionatesOxidoreductasesGene DeletionLactobacillus plantarumFood ScienceBiotechnologyApplied and Environmental Microbiology
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Competitive Binding of Aroma Compounds by β-Cyclodextrin

2001

Retention of six aroma compounds has been studied after dehydration of ternary mixtures of aroma water and beta-cyclodextrin. A maximal retention of a mole of aroma per mole of beta-cyclodextrin has been observed for five of the aroma compounds, whereas retention of benzyl alcohol can be twice as high. Retention of a mixture of aroma compounds has also been studied. It has been noted that when volatile compounds compete for the same binding sites on beta-cyclodextrin, ethyl hexanoate, 2-methylbutyric acid, and benzyl alcohol are, respectively, better retained than ethyl propionate, hexanoic acid, and hexanol. Preferential retention observed with esters can be simply explained by their diffe…

Carboxylic AcidsAlcoholBinding Competitivechemistry.chemical_compoundEthyl propionateOrganic chemistryAromachemistry.chemical_classificationHexanoic acidCyclodextrinsCyclodextrinbiologybeta-Cyclodextrinsfood and beveragesEthyl hexanoateEstersGeneral Chemistrybiology.organism_classificationKineticsFreeze DryingchemistryBenzyl alcoholAlcoholsOdorantsGeneral Agricultural and Biological SciencesHexanolJournal of Agricultural and Food Chemistry
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Analysis of Organic Aerosols Using a Micro-Orifice Volatilization Impactor Coupled to an Atmospheric-Pressure Chemical Ionization Mass Spectrometer

2014

We present the development and characterization of a combination of a micro-orifice volatilization impactor (MOVI) and an ion trap mass spectrometer (IT/MS) with an atmospheric-pressure chemical ionization (APCI) source. The MOVI is a multi-jet impactor with 100 nozzles, allowing the collection of aerosol particles by inertial impaction on a deposition plate. The pressure drop behind the nozzles is approximately 5%, resulting in a pressure of 96 kPa on the collection surface for ambient pressures of 101.3 kPa. The cut-point diameter (diameter of 50% collection efficiency) is at 0.13 μm for a sampling flow rate of 10 L min–1. After the collection step, aerosol particles are evaporated by he…

Carboxylic AcidsAnalytical chemistryAtmospheric-pressure chemical ionizationMass spectrometryMass SpectrometryOzoneHumansRelative humiditySpectroscopyBicyclic MonoterpenesAerosolsIonsChemical ionizationChromatographyTerpenesChemistryGeneral MedicineAtomic and Molecular Physics and OpticsAerosolAtmospheric PressureDeposition (aerosol physics)MonoterpenesAerosol mass spectrometryIon trapVolatilizationOxidation-ReductionEuropean Journal of Mass Spectrometry
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Highly efficient separation of amines by electrokinetic chromatography using resorcarene-octacarboxylic acids as pseudo-stationary phases

1998

Abstract Resorcarene-octacarboxylic acids, macrocyclic molecules built up by four alkylidene-bridged resorcinol units, were synthesized and used as pseudostationary phases in electrokinetic chromatography (EKC). Resorcarenes provide a stable structure and good solubility in electrolytes even with organic modifiers. The high electrophoretic mobility of the resorcarene-octacarboxylic acids introduced here as pseudostationary phases is based on the eight partly deprotonated carboxylic groups. This offers a broad migration time window, which is the main parameter for the resolution of peaks. From three compounds with different alkyl chain lengths (C 1 , C 5 , C 11 ), the C 11 -resorcarene-octa-…

Carboxylic acidClinical BiochemistryKineticsCarboxylic AcidsResorcinolElectrochemistryHigh-performance liquid chromatographyBiochemistryMicellar electrokinetic chromatographyAnalytical ChemistryHomologous serieschemistry.chemical_compoundElectrokinetic phenomenaColumn chromatographyDrug DiscoveryElectrochemistryAminesDerivatizationMolecular BiologyAlkylchemistry.chemical_classificationPharmacologyChromatographyChromatographyElutionHydrophilic interaction chromatographyOrganic ChemistryResorcinolsGeneral MedicineCapacity factorKineticschemistryChromatography columnBiomedical Chromatography
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Human HepG2 and rat Fao hepatic-derived cell lines show different responses to ciprofibrate, a peroxisome proliferator: analysis by flow cytometry.

1996

Abstract Peroxisome proliferators, and especially hypolipidemic drugs such as ciprofibrate, are known to be hepatocarcinogens in rodents, but their effect in humans is controversial. In an attempt to investigate the effects of ciprofibrate at a cellular level, the analysis of individual whole cells was performed by flow cytometry on samples from two hepatic-derived cell lines: the rat Fao cell line and the human HepG2 cell line. The increase of light scatter signals in rat Fao cells treated for 3 days with ciprofibrate at 250 μMwas related to modifications of intrinsic cellular parameters, such as size and cytoplasmic granularity. Conversely, no variations appeared in human HepG2-treated ce…

Carcinoma HepatocellularLightPeroxisome ProliferationBiologyCytoplasmic GranulesMicrobodiesFlow cytometryClofibric AcidmedicineTumor Cells CulturedAnimalsHumansScattering RadiationCell SizeHypolipidemic Agentschemistry.chemical_classificationOxidase testmedicine.diagnostic_testCell CycleLiver NeoplasmsFibric AcidsCell BiologyDNA NeoplasmCell cycleFlow CytometryCell biologyRatsEnzymeBiochemistrychemistryLiverCytoplasmCell cultureCiprofibrateOxidoreductasesCell Divisionmedicine.drugExperimental cell research
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Stimulation of peroxisomal palmitoyl-CoA oxidase activity by ciprofibrate in hepatic cell lines: comparative studies in Fao, MH1C1 and HepG2 cells.

1993

The response of two rat cell lines, Fao and MH1C1, and one human cell line, HepG2, to the peroxisome proliferator ciprofibrate, was studied. Using a fluorometric assay for palmitoyl-CoA oxidase, the dose- and time-dependent increase of this enzymatic activity was determined. From the lowest concentration (100 microM) stimulation is evident in the two rat cell lines. In the Fao line, the activity was stimulated reaching a seven-fold increase over the control level at 250 microM after 72 h of treatment. In the MH1C1 line, the maximum stimulation, four- to five-fold, was obtained at 250 and 500 microM after 72 h. In the HepG2 cell line, activity increased two-fold at 250 microM after 72 h reac…

Carcinoma HepatocellularStimulationBiologyMicrobodiesClofibric AcidLiver Neoplasms ExperimentalmedicineTumor Cells CulturedAcyl-CoA oxidaseAnimalsHumansHypolipidemic AgentsOxidase testLiver NeoplasmsFibric AcidsCell BiologyGeneral MedicinePeroxisomePalmitoyl-CoA oxidase activityBiochemistryLiverCell cultureHepatic stellate cellCiprofibrateOxidoreductasesmedicine.drugBiology of the cell
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Cytotoxic effects and degradation products of three mycotoxins: Alternariol, 3-acetyl-deoxynivalenol and 15-acetyl-deoxynivalenol in liver hepatocell…

2015

This work is focused in studying the cytotoxic effects on HepG2 cells of the mycotoxins alternariol (AOH), 3-acetyl-deoxynivalenol (3-ADON) and 15-acetyl-deoxynivalenol (15-ADON) by the MTT assay, as well as in the identification of the degradation products and/or metabolites originated after treatment by liquid chromatography tandem mass spectrometry (LC-MS/MS) equipment and extracted from culture media. HepG2 cells were treated at different concentrations over 24, 48 and 72 h. The IC50 values were from 65 to 96 μM, from 3.6 to 6.2 μM and from 5.2 to 8.1 μM for AOH, 3-ADON and 15-ADON, respectively. Among all three mycotoxins assayed, deoxynivalenol (DON) derivated presented the highest to…

Carcinoma HepatocellularTime FactorsCell SurvivalAlternariolToxicologyMass spectrometryInhibitory Concentration 50Lactoneschemistry.chemical_compoundTandem Mass SpectrometryLiquid chromatography–mass spectrometryHumansMTT assayCysteineMycotoxinBiotransformationChromatography Reverse-PhaseChromatographyDose-Response Relationship DrugLiver NeoplasmsHep G2 CellsGeneral MedicineGlutathioneSulfuric AcidsGlutathionechemistryTrichothecenesConjugateCysteineToxicology Letters
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Impact of high-fat diet on antioxidant status, vascular wall thickening and cardiac function in adult female LDLR<sup>–/–</sup> mice

2012

International audience; Background: Western diet, rich in saturated fatty acids and cholesterol, is associated with increased cardiovascular risk. We thus investigated in female mice the influence of this diet on plasma antioxidant status, vascular wall thickening and cardiac function. Methods and Results: Adult female C57BL/6J wild type (WT) and LDLR–/– mice were fed a normal diet (ND) or a high-fat diet (HFD) for 17 weeks. HFD induced an increase in plasma lipids and vitamin C (Vit C) levels in both groups but at a much higher level in LDLR–/– and a decrease in plasma ascorbyl free radical levels to Vit C ratio (an endogenous oxidative stress index) in LDLR–/–. We only found a slight decr…

Cardiac function curveAortic archmedicine.medical_specialtyAntioxidantOxygen radical absorbance capacityNormal dietAscorbyl Free Radicalmedicine.medical_treatment030204 cardiovascular system & hematologymedicine.disease_cause03 medical and health scienceschemistry.chemical_compound0302 clinical medicine[SDV.MHEP.CSC]Life Sciences [q-bio]/Human health and pathology/Cardiology and cardiovascular systemInternal medicinemedicine.arterymedicineVitamin C030304 developmental biologySystolic Function0303 health sciencesOxygen Radical Absorbance CapacityAortic ArchVitamin CCholesterolbusiness.industryOxidant/Antioxidant StatusHigh-Fat Dietfood and beveragesnutritional and metabolic diseases3. Good healthSurgeryEndocrinologychemistryEchocardiographylipids (amino acids peptides and proteins)businessOxidative stress
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The influence of atorvastatin on parameters of inflammation left ventricular function, hospitalizations and mortality in patients with dilated cardio…

2013

Background: We assessed the influence of atorvastatin on selected indicators of an inflammatory condition, left ventricular function, hospitalizations and mortality in patients with dilated cardiomyopathy (DCM). Methods. We included 68 DCM patients with left ventricular ejection fraction (LVEF) ≤40% treated optimally in a prospective, randomized study. They were observed for 5 years. Patients were divided into two groups: patients who were commenced on atorvastatin 40 mg daily for two months followed by an individually matched dose of 10 or 20 mg/day (group A), and patients who were treated according to current recommendations without statin therapy (group B). Results: After 5-year follow-u…

Cardiomyopathy DilatedMalemedicine.medical_specialtyStatinmedicine.drug_classAtorvastatinEndocrinology Diabetes and MetabolismClinical BiochemistryDiastoleCardiomyopathyDilated cardiomyopathyHemodynamicsHeart failureAtorvastatin Dilated cardiomyopathy Heart failure InflammationVentricular Function LeftEndocrinologyInternal medicinemedicineAtorvastatinHumansPyrrolescardiovascular diseasesAgedBiochemistry medicalInflammationEjection fractionbusiness.industryResearchBiochemistry (medical)Anti-Inflammatory Agents Non-SteroidalDilated cardiomyopathyMiddle Agedmedicine.diseaseUric AcidHospitalizationHeptanoic AcidsHeart failureCardiologyCytokinesFemalebusinessmedicine.drugFollow-Up StudiesLipids in health and disease
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