0000000000243625
AUTHOR
Günter Behr
Influence of growth parameters and melt convection on the solid-liquid interface during RF-floating zone crystal growth of intermetallic compounds
Abstract The influence of growth parameters and melt convection on the solid–liquid interface of the intermetallic compound Ni3Si grown by the RF-floating zone technique was investigated experimentally as well as numerically. Numerical simulations showed that the heat transfer is strongly influenced by the electromagnetically driven and Marangoni convections whereas both the buoyancy and feed rotation have a negligible effect. It was found experimentally that the inductor design, the rod diameter and the length of the molten zone influence the solid–liquid interface shape significantly. The electromagnetically driven convection increases dramatically with increasing zone length due to the r…
Magnetic field controlled FZ single crystal growth of intermetallic compounds
Abstract Intermetallic rare-earth-transition-metal compounds with their coexistence of magnetic ordering and superconductivity are still of great scientific interest. The crystal growth of bulk single crystals is very often unsuccessful due to an unfavorable solid–liquid interface geometry enclosing concave fringes. The aim of the work is the contactless control of heat and material transport during floating-zone single crystal growth of intermetallic compounds. This control is provided by a tailored design of the electromagnetic field and the resulting electromagnetically driven convection. Numerical simulations for the determination of the electromagnetic field configuration induced by th…