0000000000341941

AUTHOR

Vincenza Crupi

0000-0003-3545-6289

showing 7 related works from this author

Multi-Technique Diagnostic Investigation in View of the Restoration of “The Glory of St. Barbara” Painting by Mattia Preti

2022

The present paper illustrates the results of a diagnostic investigation performed on the oil on canvas painting “The Glory of St. Barbara” (1680–1688) by Mattia Preti. The painting is located inside the St. Barbara Church in Taverna (Catanzaro, Italy), the city that gave birth to the artist. In situ, non-invasive studies, by applying X-ray fluorescence (XRF) spectroscopy, along with laboratory micro-destructive analytical investigations, by employing electron probe microanalyses (EPMA) coupled with energy-dispersive spectrometry (EDS) and micro-Raman (µ-Raman) spectroscopy, were combined to retrieve the color palette and identify the painting technique and style of t…

TechnologyrestorationQH301-705.5pigmentsQC1-999multi-methodological approachMattia Preti Multi‐methodological approach Palette Pigments Restorationmulti-methodological approach; Mattia Preti; palette; pigments; restorationMattia Preti; Multi‐methodological approach; Palette; Pigments; RestorationGeneral Materials ScienceBiology (General)InstrumentationQD1-999Settore GEO/09 -Georis. Miner.e Appl.Mineral.-Petrogr. per l'Ambi.ed i B.Cult.Fluid Flow and Transfer ProcessespaletteProcess Chemistry and TechnologyMulti‐methodological approachTPhysicsGeneral EngineeringEngineering (General). Civil engineering (General)Computer Science ApplicationsMattia PretiChemistryTA1-2040Applied Sciences
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Multitechnique diagnostic analysis and 3D surveying prior to the restoration of St. Michael defeating Evil painting by Mattia Preti

2021

In this study, a multimethodological analysis involving optical and physical/chemical diagnostic techniques and 3D photogrammetric survey was successfully applied, for the first time, on the large oil on canvas St. Michael defeating Evil painting by Mattia Preti, located inside the Church of the Immaculate Conception of Sarria (Floriana) in Malta. Pigmenting agents, binder media, and raw materials were first characterized, both at elemental and molecular scales, through X-ray fluorescence spectroscopy (XRF), optical stereo microscopy (SM), scanning electron microscopy coupled with energy dispersive X-ray spectroscopy (SEM-EDX), Fourier transform infrared spectroscopy (FT-IR), and gas chroma…

PaintingHealth Toxicology and MutagenesisOil paintingmedia_common.quotation_subject3D photogrammetric survey Conservation Globigerina limestone Lunette Mattia Preti Multitechnique analysis Pigment’s identificationSpectrometry X-Ray Emissiongovernment.political_districtGeneral MedicineArtPollutionSt. MichaelPalette (painting)PhotogrammetryDiagnostic analysisComputer graphics (images)Spectroscopy Fourier Transform InfraredMicroscopy Electron ScanninggovernmentEnvironmental ChemistryPaintingsPIGMENTING AGENTSSettore GEO/09 -Georis. Miner.e Appl.Mineral.-Petrogr. per l'Ambi.ed i B.Cult.media_commonEnvironmental Science and Pollution Research
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Archaeometric Characterisation of Decorated Pottery from the Archaeological Site of Villa dei Quintili (Rome, Italy): Preliminary Study

2019

This work focused on the study of decorated pottery dated back to the 16th century from the Roman archaeological site of Villa dei Quintili, a monumental complex located in the south-eastern part of Rome (Italy). A minero-petrographic and geochemical study was undertaken to analyse five archaeological samples in order to define textural features and raw materials used for their production, along with the chemical and physical composition of the superficial decorative glazed coatings. For this purpose, different analytical methods were used, such as polarising optical microscope (POM), X-ray diffraction (XRD), micro-Raman spectroscopy, X-Ray fluorescence (XRF), and electron microprobe analys…

media_common.quotation_subject02 engineering and technologypetrographyPetrographyMajolica0601 history and archaeologymicro-Raman spectroscopySettore GEO/09 -Georis. Miner.e Appl.Mineral.-Petrogr. per l'Ambi.ed i B.Cult.Decorative glazed coatingmedia_common060102 archaeologyDecorative glazed coatings EMPA-EDS Micro-Raman spectroscopy Petrography Potterylcsh:QE1-996.5EMPA-EDSThe Renaissance06 humanities and the artsArtpottery021001 nanoscience & nanotechnologyArchaeologyMicro raman spectroscopylcsh:GeologyEnergy dispersive spectrometrydecorative glazed coatingsGeneral Earth and Planetary SciencesPottery0210 nano-technologyEarth and Planetary Sciences (all)
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Quasi-elastic light scattering in polymer-containing microemulsion

1996

Abstract Quasi-elastic light scattering (QELS) was performed in dilute water in oil microemulsion stabilized by AOT surfactant. The water-soluble polyethylene oxide (PEO) with low molecular weight (8000) added to the microemulsion seems to be confined within the aqueous microphase, since PEO is insoluble in oil (n-heptane). The measurements by QELS of diffusion coefficient, at dilute concentrations, allow determination of the size of the droplets. The phase diagram of the microemulsion undergoes remarkable changes on addition of the polymer. The results show that at fixed R ( water surfactant ratio) the droplets decrease their size as the concentration of polymer increases. This occurrence …

chemistry.chemical_classificationAqueous solutionChromatographyHydrodynamic radiusDiffusionOrganic Chemistrytechnology industry and agriculturePolymerLight scatteringAnalytical ChemistryInorganic ChemistryReduced propertieschemistryPulmonary surfactantChemical engineeringMicroemulsionSpectroscopyJournal of Molecular Structure
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Evaluating the protecting effects of two consolidants applied on Pietra di Lecce limestone: A neutronographic study

2020

Abstract In this work a combined laboratory-based and neutronographic investigation was carried out on a type of limestone, known as Pietra di Lecce stone, widely used in Italian Baroque as construction material. The limestone was treated with two different commercially-available coatings, namely nanosilica and nanolime, and artificially weathered by salt crystallization and temperature/relative humidity jumps. The aim was to provide an experimental evidence of the protective and consolidating effectiveness of the two treatments by looking at the water absorption process occurring inside the pore network of the analyzed stones. The analysis of the wetting front position revealed significant…

Consolidants Limestone Neutronography Sorptivity Water kineticsArcheologyAbsorption of waterMaterials scienceMaterials Science (miscellaneous)Mineralogy02 engineering and technologyConservation01 natural sciencesWater kineticsConsolidantsConsolidantSorptivityRelative humidityConsolidants; Limestone; Neutronography; Sorptivity; Water kineticsSpectroscopySalt crystallizationSettore GEO/09 -Georis. Miner.e Appl.Mineral.-Petrogr. per l'Ambi.ed i B.Cult.010401 analytical chemistryWetting front021001 nanoscience & nanotechnologyLimestone0104 chemical sciencesChemistry (miscellaneous)0210 nano-technologyGeneral Economics Econometrics and FinanceNeutronography
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New insights to assess the consolidation of stone materials used in built heritage: the case study of ancient graffiti (Tituli Picti) in the archaeol…

2020

AbstractTituli Picti are an ancient form of urban graffiti very common in the archaeological site of Pompeii (Naples, South—Italy). They are generally made of red pigments applied on walls of Campanian ignimbrite. This paper deals with a scientific investigation aimed to their conservation. This is a challenging task since it requires a multidisciplinary approach that includes restorers, archaeologists and conservation scientists. The study has provided suggestions on the proper way to conserve Tituli Picti over time. In the present work, several specimens of Campanian ignimbrite were painted with red earth pigment; lime and Arabic gum have been used as binders as well. Such painted stones …

Archeologylcsh:QD71-142lcsh:Fine ArtsConsolidation (soil)Conservation Consolidation Tituli Picti of PompeiiArabicTituli Picti of Pompeii010401 analytical chemistrylcsh:Analytical chemistryThermal agingConservationTituli Picti of Pompeii Conservation Consolidation010502 geochemistry & geophysicsGraffiti01 natural sciencesArchaeologylanguage.human_language0104 chemical sciencesScotch tapelanguagelcsh:NBuilt heritageSettore GEO/09 -Georis. Miner.e Appl.Mineral.-Petrogr. per l'Ambi.ed i B.Cult.Consolidation0105 earth and related environmental sciences
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Additional file 1 of New insights to assess the consolidation of stone materials used in built heritage: the case study of ancient graffiti (Tituli P…

2020

Additional file 1: Table S1. Summary of the consolidation treatments carried out on the painted specimens. Figure S1. Arrangement of the washout test, samples were immersed in deionized water and a vortex were generated by means of a magnetic stirrer.

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