0000000000371233
AUTHOR
Sobhy E. Elsilk
showing 2 related works from this author
Synthesis, crystal structure, DFT and biological activity of E-pyrene-1-carbaldehyde oxime and E-2-naphthaldehyde oxime
2020
Abstract The aldoximes E-pyrene-1-carbaldehyde oxime 1 and E-2-naphthaldehyde oxime 2 were synthesized, in ca. 90% yield, by treatment of pyrene-1-carbaldehyde or 2-naphthaldehyde, respectively, with hydroxylamine hydrochloride and sodium carbonate in MeOH. Compounds 1 and 2 were characterized by IR, 1H and 13C{1H} NMR spectroscopies, elemental analyses and single crystal X-ray diffraction (in the case of 1). The studied system (compound 1) showed significant amounts of H⋯H (44.4%), C⋯H (25.4%) and C⋯C (13.3%) intermolecular interactions in addition to the short N⋯H (5.9%) and O⋯H (6.2%) intermolecular interactions. These interactions affect the molecular packing of the studied system in th…
CCDC 1970751: Experimental Crystal Structure Determination
2020
Related Article: Jamal Lasri, Saied M. Soliman, Sobhy E. Elsilk, Matti Haukka, Ayman El-Faham|2020|J.Mol.Struct.|1207|127848|doi:10.1016/j.molstruc.2020.127848