0000000000395277
AUTHOR
Guillermo Minguez Espallargas
Synthesis, Structures, and Solution Studies of a New Class of [Mo2O2S2]-Based Thiosemicarbazone Coordination Complexes
This paper deals with the synthesis, structural studies, and behavior in solution of unprecedented coordination complexes built by the association of a panel of 14 representative thiosemicarbazone ligands with the cluster [Mo2O2S2]2+. These complexes have been thoroughly characterized both in the solid state and in solution by XRD and by NMR, respectively. In particular, HMBC 1H{15N} and 1H DOSY NMR experiments bring important elements for understanding the complexes' behavior in solution. These studies demonstrate that playing on the nature and the position of various substituents on the ligands strongly influences the coordination modes of the ligands as well as the numbers of isomers in …
CCDC 1830490: Experimental Crystal Structure Determination
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CCDC 1830489: Experimental Crystal Structure Determination
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CCDC 1853491: Experimental Crystal Structure Determination
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CCDC 1899778: Experimental Crystal Structure Determination
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CCDC 2091526: Experimental Crystal Structure Determination
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