Author: M. Bujak

0000000000445285

AUTHOR

M. Bujak

Phase transition in bis(ethyldimethylammonium) pentachloroantimonate(III)

The crystal structure of a new member of the alkylammonium chloroantimonate family, namely bis-(ethyldimethylammonium) pentachloroantimonate(III), [C 2 H 5 NH(CH 3 ) 2 ] 2 [SbCl 5 ], was determined at room temperature. The anionic sublattice consists of isolated distorted square-pyramidal [SbCl 5 ] 2- units and two crystallographically inequivalent disordered ethyldimethylammonium cations connected to anions by NH...Cl hydrogen bonds. The disorder is realised by the presence of two positions for all C, N and H atoms, and is explained as being a result of the overall reorientation of cations along the long axis of the molecule. One second-order phase transition was found at ca 160 K and resu…

0000000000445285

AUTHOR

M. Bujak

Phase transition in bis(ethyldimethylammonium) pentachloroantimonate(III)

Bis(dimethylammonium) pentachloroantimonate(III), on the deformation of the octahedral coordination of Sb III

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