0000000000445286
AUTHOR
J. Zaleski
Phase transition in bis(ethyldimethylammonium) pentachloroantimonate(III)
The crystal structure of a new member of the alkylammonium chloroantimonate family, namely bis-(ethyldimethylammonium) pentachloroantimonate(III), [C 2 H 5 NH(CH 3 ) 2 ] 2 [SbCl 5 ], was determined at room temperature. The anionic sublattice consists of isolated distorted square-pyramidal [SbCl 5 ] 2- units and two crystallographically inequivalent disordered ethyldimethylammonium cations connected to anions by NH...Cl hydrogen bonds. The disorder is realised by the presence of two positions for all C, N and H atoms, and is explained as being a result of the overall reorientation of cations along the long axis of the molecule. One second-order phase transition was found at ca 160 K and resu…
Relationship Between Anti-DFS70 Autoantibodies and Oxidative Stress
Background: The anti-DFS70 autoantibodies are one of the most commonly and widely described agent of unknown clinical significance, frequently detected in healthy individuals. It is not known whether the DFS70 autoantibodies are protective or pathogenic. One of the factors suspected of inducing the formation of anti-DFS70 antibodies is increased oxidative stress. We evaluated the coexistence of anti-DFS70 antibodies with selected markers of oxidative stress and investigated whether these antibodies could be considered as indirect markers of oxidative stress. Methods: The intensity of oxidative stress was measured in all samples via indices of free-radical damage to lipids and proteins such …
1H NMR study of dynamical inequivalence of cations in [C(NH2)3]3Sb2Cl9
Abstract The proton NMR second moment and spin–lattice relaxation time have been studied for polycrystalline tris-guanidinium nonachlorodiantimonate(III) in a wide temperature range. The C 3 reorientation of two types of the cations, hindered by very different potential barriers (20.5 and 54.5 kJ/mol) has been revealed. An unusually large dynamical inequivalence of two cations evidently reflects their different crystalline environments.
Bis(dimethylammonium) pentachloroantimonate(III), on the deformation of the octahedral coordination of Sb III
The structure of the title compound, [NH2(CH3)2]2SbCl5, was determined at 295 and 85 K. It consists of polymeric (SbCl52−)n chains composed of deformed SbCl63− octahedra connected by corners and dimethylammonium cations. The temperature dependence of the Sb–Cl bond lengths is discussed. It is argued that the deformation of the octahedral coordination of the SbIII atom is caused by electrostatic interaction/hydrogen bonds.
Lipid levels, atrial fibrillation and the impact of age:Results from the LIPIDOGRAM2015 study
Background and aims: An inverse relationship between lipid levels and atrial fibrillation (AF) has been suggested, but whether the association is upheld for all age groups remains unclear. The aim of the study was to examine associations between lipid levels and AF by age groups in a nationwide study in Poland. Methods: Multivariate Poisson regression models were used to estimate prevalence ratios (PRs) for AF by lipid levels. Low-density lipoprotein cholesterol (LDL-C), high-density lipoprotein cholesterol (HDL-C), triglycerides (TG), total cholesterol (TC), non-HDL-C and LDL-C/HDL-C ratios were grouped into quartiles. Results: Of the 13,724 participants, 5.2% (n = 708) had AF. People with…
CCDC 652130: Experimental Crystal Structure Determination
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CCDC 224657: Experimental Crystal Structure Determination
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CCDC 166998: Experimental Crystal Structure Determination
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CCDC 141924: Experimental Crystal Structure Determination
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CCDC 146061: Experimental Crystal Structure Determination
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CCDC 189320: Experimental Crystal Structure Determination
Related Article: M.Wojtas, G.Bator, R.Jakubas, J.Zaleski, B.Kosturek, J.Baran|2003|J.Solid State Chem.|173|425|doi:10.1016/S0022-4596(03)00137-3
CCDC 138020: Experimental Crystal Structure Determination
Related Article: M.Bujak, J.Zaleski|1999|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|55|1775|doi:10.1107/S0108270199009464
CCDC 255863: Experimental Crystal Structure Determination
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CCDC 614863: Experimental Crystal Structure Determination
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CCDC 638333: Experimental Crystal Structure Determination
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CCDC 160134: Experimental Crystal Structure Determination
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CCDC 135826: Experimental Crystal Structure Determination
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CCDC 163934: Experimental Crystal Structure Determination
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CCDC 183946: Experimental Crystal Structure Determination
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CCDC 607733: Experimental Crystal Structure Determination
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CCDC 631908: Experimental Crystal Structure Determination
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CCDC 270367: Experimental Crystal Structure Determination
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CCDC 251305: Experimental Crystal Structure Determination
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CCDC 163897: Experimental Crystal Structure Determination
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CCDC 195616: Experimental Crystal Structure Determination
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CCDC 141923: Experimental Crystal Structure Determination
Related Article: M.Bujak, L.Sikorska, J.Zaleski|2000|Z.Anorg.Allg.Chem.|626|2535|doi:10.1002/1521-3749(200012)626:12<2535::AID-ZAAC2535>3.0.CO;2-U
CCDC 257220: Experimental Crystal Structure Determination
Related Article: P.Szklarz, J.Zaleski, R.Jakubas, G.Bator, W.Medycki, K.Falinska|2005|J.Phys.:Condens.Matter|17|2509|doi:10.1088/0953-8984/17/15/021
CCDC 268089: Experimental Crystal Structure Determination
Related Article: J.Zaleski, M.Gabryszewski, B.Zarychta|2005|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|61|m151|doi:10.1107/S0108270105003446
CCDC 162577: Experimental Crystal Structure Determination
Related Article: J.Zaleski, Z.Daszkiewicz, J.B.Kyziol|2001|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|57|304|doi:10.1107/S0108270100019144
CCDC 1565676: Experimental Crystal Structure Determination
Related Article: A. Jezuita, G. Spaleniak, K. Ejsmont, J. Zaleski, B. Zarychta|2017|IUCrData|2|x171121|doi:10.1107/S241431461701121X
CCDC 669137: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, J.Zaleski|2007|Acta Crystallogr.,Sect.E:Struct.Rep.Online|63|o4315|doi:10.1107/S1600536807049690
CCDC 130749: Experimental Crystal Structure Determination
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CCDC 160007: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, M.Makowski, J.Zaleski|2001|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|57|205|doi:10.1107/S0108270100017753
CCDC 251306: Experimental Crystal Structure Determination
Related Article: J.Zaleski, G.Spaleniak, J.B.Kyziol|2004|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|60|o627|doi:10.1107/S0108270104001428
CCDC 180196: Experimental Crystal Structure Determination
Related Article: J.Zaleski, Z.Daszkiewicz, J.Kyziol|2002|Acta Crystallogr.,Sect.B:Struct.Sci.|58|109|doi:10.1107/S0108768101016548
CCDC 618777: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, J.Zaleski|2006|Acta Crystallogr.,Sect.E:Struct.Rep.Online|62|o3386|doi:10.1107/S1600536806026948
CCDC 234051: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, A.A.Domanski, J.B.Kyziol, J.Zaleski|2005|J.Mol.Struct.|753|92|doi:10.1016/j.molstruc.2005.05.045
CCDC 130750: Experimental Crystal Structure Determination
Related Article: M.Bujak, J.Zaleski|1998|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|54|1773|doi:10.1107/S0108270198008865
CCDC 182020: Experimental Crystal Structure Determination
Related Article: M.Bujak, J.Zaleski, V.Prezhdo, B.Uspenskiy|2002|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|58|o76|doi:10.1107/S0108270101019539
CCDC 611080: Experimental Crystal Structure Determination
Related Article: D.Siodlak, A.Macedowska-Capiga, K.Ejsmont, J.Zaleski, B.Rzeszotarska|2007|Z.Kristallogr.|222|297|doi:10.1524/zkri.2007.222.6.297
CCDC 157094: Experimental Crystal Structure Determination
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CCDC 208515: Experimental Crystal Structure Determination
Related Article: M.Wojtas, G.Bator, R.Jakubas, J.Zaleski|2003|J.Phys.:Condens.Matter|15|5765|doi:10.1088/0953-8984/15/33/310
CCDC 130693: Experimental Crystal Structure Determination
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CCDC 246773: Experimental Crystal Structure Determination
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CCDC 163896: Experimental Crystal Structure Determination
Related Article: M.Bujak, P.Osadczuk, J.Zaleski|2001|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|57|388|doi:10.1107/S0108270101000774
CCDC 640267: Experimental Crystal Structure Determination
Related Article: J.B.Kyziol, J.Zaleski|2007|Acta Crystallogr.,Sect.E:Struct.Rep.Online|63|o1235|doi:10.1107/S160053680700339X
CCDC 282214: Experimental Crystal Structure Determination
Related Article: B.Zarychta, A.Piecyk-Mizgala, Z.Daszkiewicz, J.Zaleski|2005|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|61|o515|doi:10.1107/S010827010502158X
CCDC 164033: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, M.Wasielewski, J.Zaleski|2002|Acta Crystallogr.,Sect.E:Struct.Rep.Online|58|m200|doi:10.1107/S1600536802006402
CCDC 268090: Experimental Crystal Structure Determination
Related Article: J.Zaleski, M.Gabryszewski, B.Zarychta|2005|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|61|m151|doi:10.1107/S0108270105003446
CCDC 257221: Experimental Crystal Structure Determination
Related Article: P.Szklarz, J.Zaleski, R.Jakubas, G.Bator, W.Medycki, K.Falinska|2005|J.Phys.:Condens.Matter|17|2509|doi:10.1088/0953-8984/17/15/021
CCDC 235773: Experimental Crystal Structure Determination
Related Article: M.Bujak, J.Zaleski|2004|J.Solid State Chem.|177|3202|doi:10.1016/j.jssc.2004.05.036
CCDC 166997: Experimental Crystal Structure Determination
Related Article: J.Zaleski, Z.Daszkiewicz, J.B.Kyziol|2001|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|57|754|doi:10.1107/S0108270101004784
CCDC 135825: Experimental Crystal Structure Determination
Related Article: M.Bujak, P.Osadczuk, J.Zaleski|1999|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|55|1443|doi:10.1107/S0108270199008264
CCDC 222871: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, J.Zaleski, A.Sporzynski, M.Lewandowski|2003|Acta Crystallogr.,Sect.E:Struct.Rep.Online|59|o1324|doi:10.1107/S1600536803017999
CCDC 241244: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, A.A.Domanski, J.B.Kyziol, J.Zaleski|2004|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|60|o368|doi:10.1107/S0108270104007103
CCDC 611081: Experimental Crystal Structure Determination
Related Article: D.Siodlak, A.Macedowska-Capiga, K.Ejsmont, J.Zaleski, B.Rzeszotarska|2007|Z.Kristallogr.|222|297|doi:10.1524/zkri.2007.222.6.297
CCDC 235774: Experimental Crystal Structure Determination
Related Article: M.Bujak, J.Zaleski|2004|J.Solid State Chem.|177|3202|doi:10.1016/j.jssc.2004.05.036
CCDC 208514: Experimental Crystal Structure Determination
Related Article: M.Wojtas, G.Bator, R.Jakubas, J.Zaleski|2003|J.Phys.:Condens.Matter|15|5765|doi:10.1088/0953-8984/15/33/310
CCDC 195617: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, M.Broda, A.Domanski, J.B.Kyziol, J.Zaleski|2002|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|58|o545|doi:10.1107/S0108270102011952
CCDC 163935: Experimental Crystal Structure Determination
Related Article: A.Domanski, K.Ejsmont, J.B.Kyziol, J.Zaleski|2001|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|57|467|doi:10.1107/S0108270101000518
CCDC 224650: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, J.Zaleski, I.H.Joe, V.S.Jayakumar|2003|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|59|o553|doi:10.1107/S0108270103018031
CCDC 630451: Experimental Crystal Structure Determination
Related Article: J.B.Kyziol, P.Nogly, Z.Daszkiewicz, J.Zaleski|2006|Acta Crystallogr.,Sect.E:Struct.Rep.Online|62|o5485|doi:10.1107/S1600536806045946
CCDC 217617: Experimental Crystal Structure Determination
Related Article: B.Zarychta, J.Zaleski, B.Gawdzik, W.Iwanek|2003|Acta Crystallogr.,Sect.E:Struct.Rep.Online|59|o1055|doi:10.1107/S160053680301393X
CCDC 830703: Experimental Crystal Structure Determination
Related Article: B.Zarychta, J.Zaleski, J.Kyziol, Z.Daszkiewicz, C.Jelsch|2011|Acta Crystallogr.,Sect.B:Struct.Sci.|67|250|doi:10.1107/S0108768111013140
CCDC 641724: Experimental Crystal Structure Determination
Related Article: J.B.Kyziol, E.M.Nowakowska, J.Zaleski|2007|Acta Crystallogr.,Sect.E:Struct.Rep.Online|63|o2834|doi:10.1107/S1600536807021332
CCDC 611082: Experimental Crystal Structure Determination
Related Article: D.Siodlak, A.Macedowska-Capiga, K.Ejsmont, J.Zaleski, B.Rzeszotarska|2007|Z.Kristallogr.|222|297|doi:10.1524/zkri.2007.222.6.297
CCDC 241233: Experimental Crystal Structure Determination
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CCDC 257222: Experimental Crystal Structure Determination
Related Article: P.Szklarz, J.Zaleski, R.Jakubas, G.Bator, W.Medycki, K.Falinska|2005|J.Phys.:Condens.Matter|17|2509|doi:10.1088/0953-8984/17/15/021
CCDC 611212: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, J.Zaleski|2006|Acta Crystallogr.,Sect.E:Struct.Rep.Online|62|o2512|doi:10.1107/S160053680601926X
CCDC 631907: Experimental Crystal Structure Determination
Related Article: J.Tarasiewicz, R.Jakubas, J.Zaleski, J.Baran|2008|J.Mol.Struct.|876|86|doi:10.1016/j.molstruc.2007.06.005
CCDC 691133: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, M.Zareef, M.Arfan, S.A.Bashir, J.Zaleski|2008|Acta Crystallogr.,Sect.E:Struct.Rep.Online|64|o1128|doi:10.1107/S1600536808014645
CCDC 206770: Experimental Crystal Structure Determination
Related Article: B.Zarychta, G.Spaleniak, J.Zaleski|2003|Acta Crystallogr.,Sect.E:Struct.Rep.Online|59|o304|doi:10.1107/S1600536803003027
CCDC 183945: Experimental Crystal Structure Determination
Related Article: M.Bujak, J.Zaleski|2003|J.Mol.Struct.|647|121|doi:10.1016/S0022-2860(02)00509-4
CCDC 234050: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, A.A.Domanski, J.B.Kyziol, J.Zaleski|2005|J.Mol.Struct.|753|92|doi:10.1016/j.molstruc.2005.05.045
CCDC 180197: Experimental Crystal Structure Determination
Related Article: J.Zaleski, Z.Daszkiewicz, J.Kyziol|2002|Acta Crystallogr.,Sect.B:Struct.Sci.|58|109|doi:10.1107/S0108768101016548
CCDC 153923: Experimental Crystal Structure Determination
Related Article: J.Kyziol, Z.Daszkiewicz, J.Zaleski|2000|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|56|1401|doi:10.1107/S0108270100011604
CCDC 747433: Experimental Crystal Structure Determination
Related Article: E.M.Nowakowska-Bogdan, E.Wicher, K.Ejsmont, J.Zaleski|2009|Acta Crystallogr.,Sect.E:Struct.Rep.Online|65|o2228|doi:10.1107/S1600536809032747
CCDC 160135: Experimental Crystal Structure Determination
Related Article: M.Bujak, J.Zaleski|2001|Crystal Engineering|4|241|doi:10.1016/S1463-0184(01)00018-1
CCDC 684923: Experimental Crystal Structure Determination
Related Article: J.Tarasiewicz, R.Jakubas, G.Bator, J.Zaleski, J.Baren, W.Medycki|2009|J.Mol.Struct.|932|6|doi:10.1016/j.molstruc.2009.05.034
CCDC 282213: Experimental Crystal Structure Determination
Related Article: B.Zarychta, A.Piecyk-Mizgala, Z.Daszkiewicz, J.Zaleski|2005|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|61|o515|doi:10.1107/S010827010502158X
CCDC 270368: Experimental Crystal Structure Determination
Related Article: O.Czupinski, M.Wojtas, J.Zaleski, R.Jakubas, W.Medycki|2006|J.Phys.:Condens.Matter|18|3307|doi:10.1088/0953-8984/18/12/012
CCDC 633866: Experimental Crystal Structure Determination
Related Article: M.Bujak, J.Zaleski|2007|Acta Crystallogr.,Sect.E:Struct.Rep.Online|63|m102|doi:10.1107/S1600536806051920
CCDC 274640: Experimental Crystal Structure Determination
Related Article: B.Zarychta, Z.Daszkiewicz, J.Zaleski|2005|Acta Crystallogr.,Sect.E:Struct.Rep.Online|61|o1897|doi:10.1107/S1600536805015965
CCDC 246772: Experimental Crystal Structure Determination
Related Article: R.Jakubas, B.Bednarska-Bolek, J.Zaleski, W.Medycki, K.Holderna-Natkaniec, P.Zielinski, M.Galazka|2005|Solid State Sciences|7|381|doi:10.1016/j.solidstatesciences.2005.01.010
CCDC 224656: Experimental Crystal Structure Determination
Related Article: B.Zarychta, Z.Daszkiewicz, J.B.Kyziol, J.Zaleski|2003|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|59|o564|doi:10.1107/S0108270103017888
CCDC 206783: Experimental Crystal Structure Determination
Related Article: B.Zarychta, J.Zaleski, V.Prezhdo, B.Uspenskiy|2003|Acta Crystallogr.,Sect.E:Struct.Rep.Online|59|o332|doi:10.1107/S1600536803003428
CCDC 140963: Experimental Crystal Structure Determination
Related Article: K.Ejsmont, J.Kyziol, E.Nowakowska, J.Zaleski|2000|Acta Crystallogr.,Sect.C:Cryst.Struct.Commun.|56|93|doi:10.1107/S0108270199013190