0000000000639912
AUTHOR
Stefano Legnaioli
Evaluation of Thin Film Microextraction for trace elemental analysis of liquid samples using LIBS detection
An analytical methodology based in the combination of Thin Film Microextraction with Laser-induced Breakdown Spectroscopy (TFME-LIBS) was investigated, for the first time, for detection of Cu, Cr, Ni and Pb in aqueous solutions. In this methodology, the analytes were extracted in a thin film of adsorbent material deposited on a solid support, which was introduced in the sample to analyse. After extraction, the analytes retained in the adsorbent were analysed by LIBS. In order to obtain adsorbent films useful for the microextraction step, two different experimental procedures for film generation, denoted as Drop Casting Deposition and Mould Deposition, were evaluated. In both cases, graphene…
Wood coated with plasma-polymer for water repellence
The effects of cold HMDSO and HMDSO + SF6 plasma treatments on spruce, chestnut and poplar wood were investigated in order to obtain a hydrophobic surface evaluated by microscopic, spectroscopic (FT-IR and LIBS) and contact angle analyses. Cold plasma treatments can increase the surface hydro-repellence without modifying the external aspect and bulk properties of different woods.
Social and technological changes in the ceramic production of the Northern Levant during the LBA/IA transition: New evidence about the Sea People issue through archaeometry
Abstract The transition from the Late Bronze Age (LBA) to the Iron Age (IA) in the Levant is marked by the collapse of the Egyptian and Hittite empires, which dominated the political scene of the 14th–13th century BCE. The role of the Sea People, groups of migrants who were defeated by the Egyptian king Ramses III around 1175 BCE, is the focal point concerning this period. After the collapse of the LBA empires, written sources disappeared, and the archaeologists’ primary tool to define cultural processes is to analyze the evolution of pottery. Because of this, studies about the distribution of Aegeanizing ceramic production, considered here to have derived from the Sea People culture, can p…