0000000000640401
AUTHOR
B. Abu Thaher
3-(2,4-Difluorophenyl)-1-(pyridin-4-yl)benzo[4,5]imidazo[1,2-d][1,2,4]triazin-4(3H)-one
In the title compound, C20H11F2N5O, the central 13-membered ring system (r.m.s. deviation = 0.028 Å) makes a dihedral angle of 53.13 (7)° with the difluorophenyl ring and 79.98 (7)° with the pyridine ring. The crystal packing features aromatic π–π interactions between the 13-membered rings [shortest distance between ring centroids = 3.5682 (8) Å].
Poly[[tetramethanolbis[4-oxo-3-(pyridin-4-yl)-1-(2,4,6-trichlorophenyl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-6-olato]disodium]–diethyl ether–methanol (1/1/2)]
In the title compound, [Na2(C16H7Cl3N5O2)2(CH3OH)4]·C4H10O·2CH3OH, the central pyrazolo[3,4-d]pyrimidine system makes dihedral angles of 82.98 (7)° with the trichlorophenyl ring and 13.11 (15)° with the pyridine ring. The sodium ion has an octahedral environment, being coordinated by four methanol molecules and one O and one N atom of two different heterocyclic ring systems.
CCDC 1568129: Experimental Crystal Structure Determination
Related Article: K. Wahedy, B. Abu Thaher, D. Schollmeyer, I. Almasri, R. Morjan, B. Qeshta, H.-P. Deigner|2017|Acta Crystallogr.,Sect.E:Cryst.Commun.|73|1341|doi:10.1107/S2056989017011732
CCDC 1490105: Experimental Crystal Structure Determination
Related Article: B. Abu Thaher, D. Schollmeyer, S. Laufer|2016|IUCrData|1|x161081|doi:10.1107/S2414314616010816
CCDC 1507208: Experimental Crystal Structure Determination
Related Article: B. Abu Thaher, D. Schollmeyer, B. Qeshta, K.M. Wahedy, I.M. Almasri, R.Y. Morjan, H.-P. Deigner|2016|IUCrData|1|x161529|doi:10.1107/S2414314616015297
CCDC 1568130: Experimental Crystal Structure Determination
Related Article: K. Wahedy, B. Abu Thaher, D. Schollmeyer, I. Almasri, R. Morjan, B. Qeshta, H.-P. Deigner|2017|Acta Crystallogr.,Sect.E:Cryst.Commun.|73|1341|doi:10.1107/S2056989017011732
CCDC 1501316: Experimental Crystal Structure Determination
Related Article: B. Abu Thaher, D. Schollmeyer, B. Qeshta, H.-P. Deigner|2016|IUCrData|1|x161380|doi:10.1107/S2414314616013808