0000000000749206
AUTHOR
Raimons Poplausks
Preparation and Characterization of Nanocrystalline Gadolinium Oxide Powders and Films
Due to its magnetic, electrical, absorption, and emission properties, nanoscale gadolinium oxide is widely used in various fields. In this research, nanocrystalline Gd2O3 powders and films on glass substrates have been produced by the extraction-pyrolytic method. X-ray diffraction analysis revealed the formation of single phase Gd2O3 with cubic crystal structure and the mean crystallite size from 9 to 25 nm in all produced materials. The morphology of samples has been characterized by scanning electron microscopy and transmission electron microscopy.
Hydrothermally Synthesized Strontium Peroxyapatite
The current research focuses on peroxide ion incorporation in the structure of strontium hydroxyapatite (SrHAp) by exposure to H2O2 ina closed hydrothermal vessel under mild conditions at 130 to 170 °C. Peroxide enriched strontium apatite (SrPerAp) was characterized for structure by X-Ray diffraction, for peroxide content- by permanganometric titration and then viewed by SEM. This study continued from previous work that used 30%H2O2 and showed a higher included peroxide content after processing with 50% H2O2 at 130 °C 70% of the theoretical peroxide content in apatitic channels of strontium apatite. This is the highest peroxide content incorporated to date and employs a lower temperature th…