Author: Izar Capel Berdiell

0000000000878368

AUTHOR

Izar Capel Berdiell

0000-0003-3828-7097

The effect of tether groups on the spin states of iron(ii)/bis[2,6-di(pyrazol-1-yl)pyridine] complexes

The synthesis of six 2,6-di(pyrazol-1-yl)pyridine derivatives bearing dithiolane or carboxylic acid tether groups is described: [2,6-di(pyrazol-1-yl)pyrid-4-yl]methyl (R)-lipoate (L1), 2-[(2,6-di(pyrazol-1-yl)pyridine)-4-carboxamido]ethyl (R)-lipoate (L2), 2-[(2,6-di(pyrazol-1-yl)pyridine)-4-carboxy]ethyl (R)-lipoate (L3), N-([2,6-di(pyrazol-1-yl)pyrid-4-ylsulfanyl]-2-aminoethyl (R)-lipoamide (L4), 2-[(2,6-di(pyrazol-1-yl)pyridine)-4-carboxamido]acetic acid (L5) and 2-[(2,6-di(pyrazol-1-yl)pyridine)-4-carboxamido]propionic acid (L6). The iron(ii) perchlorate complexes of all the new ligands exhibit gradual thermal spin-crossover (SCO) in the solid state above room temperature, except L4 who…

research product

CCDC 2074280: Experimental Crystal Structure Determination

Related Article: Izar Capel Berdiell, Victor García-López, Mark J. Howard, Miguel Clemente-León, Malcolm A. Halcrow|2021|Dalton Trans.|50|7417|doi:10.1039/D1DT01076J

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CCDC 2074281: Experimental Crystal Structure Determination

Related Article: Izar Capel Berdiell, Victor García-López, Mark J. Howard, Miguel Clemente-León, Malcolm A. Halcrow|2021|Dalton Trans.|50|7417|doi:10.1039/D1DT01076J

research product

CCDC 2074282: Experimental Crystal Structure Determination

Related Article: Izar Capel Berdiell, Victor García-López, Mark J. Howard, Miguel Clemente-León, Malcolm A. Halcrow|2021|Dalton Trans.|50|7417|doi:10.1039/D1DT01076J

research product

CCDC 2074283: Experimental Crystal Structure Determination

Related Article: Izar Capel Berdiell, Victor García-López, Mark J. Howard, Miguel Clemente-León, Malcolm A. Halcrow|2021|Dalton Trans.|50|7417|doi:10.1039/D1DT01076J

research product

CCDC 2074276: Experimental Crystal Structure Determination

Related Article: Izar Capel Berdiell, Victor García-López, Mark J. Howard, Miguel Clemente-León, Malcolm A. Halcrow|2021|Dalton Trans.|50|7417|doi:10.1039/D1DT01076J

research product

CCDC 2074278: Experimental Crystal Structure Determination

Related Article: Izar Capel Berdiell, Victor García-López, Mark J. Howard, Miguel Clemente-León, Malcolm A. Halcrow|2021|Dalton Trans.|50|7417|doi:10.1039/D1DT01076J

research product

CCDC 2074277: Experimental Crystal Structure Determination

Related Article: Izar Capel Berdiell, Victor García-López, Mark J. Howard, Miguel Clemente-León, Malcolm A. Halcrow|2021|Dalton Trans.|50|7417|doi:10.1039/D1DT01076J

research product

CCDC 2074279: Experimental Crystal Structure Determination

Related Article: Izar Capel Berdiell, Victor García-López, Mark J. Howard, Miguel Clemente-León, Malcolm A. Halcrow|2021|Dalton Trans.|50|7417|doi:10.1039/D1DT01076J

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