0000000000899347

AUTHOR

Cristina Prinzivalli

showing 24 related works from this author

Diorganotin(IV) N-acetyl-L-cysteinate complexes: synthesis, solid state, solution phase, DFT and biological investigations.

2009

Diorganotin(IV) complexes of N-acetyl-L-cysteine (H(2)NAC; (R)-2-acetamido-3-sulfanylpropanoic acid) have been synthesized and their solid and solution-phase structural configurations investigated by FTIR, Mössbauer, (1)H, (13)C and (119)Sn NMR spectroscopy. FTIR results suggested that in R(2)Sn(IV)NAC (R = Me, Bu, Ph) complexes NAC(2-) behaves as dianionic tridentate ligand coordinating the tin(IV) atom, through ester-type carboxylate, acetate carbonyl oxygen atom and the deprotonated thiolate group. From (119)Sn Mössbauer spectroscopy it could be inferred that the tin atom is pentacoordinated, with equatorial R(2)Sn(IV) trigonal bipyramidal configuration. In DMSO-d(6) solution, NMR spectr…

Binding SitesMolecular StructureLigandStereochemistryCell SurvivalSpectrum Analysischemistry.chemical_elementAntineoplastic AgentsNuclear magnetic resonance spectroscopyBiochemistryMedicinal chemistryAcetylcysteineCell LineInorganic Chemistrychemistry.chemical_compoundTrigonal bipyramidal molecular geometryDeprotonationchemistryMössbauer spectroscopyOrganotin CompoundsOrganotin(IV) FTIR Mössbauer NMR DFT Antitumor activityHumansDensity functional theoryCarboxylateTinJournal of inorganic biochemistry
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Synthesis, chemical characterization and biological activity of new histone acetylation/deacetylation specific inhibitors: a novel and potential appr…

2013

Three new triorganotin(IV) complexes of valproic acid (vp1, Me3Sn-valproate; vp2, Bu3Sn-valproate; vp3, Ph3Sn-valproate) have been synthesized and investigated by spectroscopic and biological methods. An anionic, monodentate valproate ligand was observed, ester-like coordinating the tin atom on a tetra-coordinated, monomeric environment. The structures, though, can distort towards a penta-coordination, as a consequence of a long range O center dot center dot center dot Sn interaction. Crystallographic and NMR findings confirm this situation both in solid state and solution. Biological finding evidenced a clear cytotoxic action of the complexes in hepatocellular carcinoma cell cultures: one …

StereochemistryCell SurvivalAntineoplastic AgentsBiochemistryInorganic ChemistryHistonesHistone H3Organotin CompoundsCytotoxic T cellHumansViability assayCells CulturedMOSSBAUER SPECTROSCOPYOrganoTin(IV)biologyX-RAY DIFFRACTIONChemistryMössbauer spectroscopyValproic AcidESI-MSBiological activityAcetylationHep G2 CellsLigand (biochemistry)NMRHistoneBiochemistryApoptosisAcetylationSettore CHIM/03 - Chimica Generale E Inorganicabiology.proteinX-ray spectroscopy
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Syntesis, characterization and electrochemistry of Ru(III) complexes with several aminoacid ligands

2007

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Synthesis, structure and electrochemistry of ruthenium(III) complexes whith potential biological activity

2007

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USO TERAPEUTICO COMBINATO DI ORGANOSTAGNO(IV) ED INIBITORI DELLE DEACETILASI ISTONICHE

2010

organostagno
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New Ruthenium complexes with antitumoral activity

2006

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Synthesis, Structural characterization and Exafs investigations of new ruthenium(III) complexes.

2008

Two new complexs of Ru(III) with glucosaminic acid and 1-Methyluracil, [RuCl2(Glun-N,O)2]H (I), (Glun-= glucosaminate); [RuCl4(1-MeU-N3)(DMSO)]H2.H2O (II), (1-MeU-= 1-Methyluracilate) were prepared from the same Ru(III) precursors, RuCl3•3H2O and [(DMSO)2H][trans-RuCl4(DMSO)2]. The characterization of the complexes have been carried out by elemental analysis, FT-IR, ES-MS, NMR and EXAFS.

Ruthenium(III) complexesFT-IR ES-MS NMR EXAFS.Settore CHIM/03 - Chimica Generale E Inorganica
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How organotin(IV)(sulfonatophenyl) porphynate may activate the apoptotic pathways in melanoma cells?

2006

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Bu2Sn(N-acetyl-L-cysteinate) antitumor activity on HepG2 cells

2010

HepG2 cellantitumor activityorganotin(IV)
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ORGANOSTAGNO(IV) COMPLESSI CON N-ACETILCISTEINA AD ATTIVITÀ ANTITUMORALE, PROCEDIMENTO PER LA LORO PRODUZIONE E LORO USO.

2008

Settore CHIM/03 - Chimica Generale E InorganicaAntitumoral organotin(IV) HepG2
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Organotin(IV) and simple fatty acids: preliminary assessments

2012

Our group has a long researching tradition in the field of organotin(IV) complexes, usually proposed and tested as potential anti-tumor drugs. The leitmotif has usually been the modulation of the intrinsic toxicity/cytotoxicity of the organometallic moiety and a modulation of the toxic effect by means of biologically related molecules (synthetic or natural). Such a modulation is usually achieved by two (often overlapping) routes: dampen the damaging effects of the metal core, and serving as a carrier for specific tissue districts. Since a too tight binding on the organotin moiety is not always desirable – a too much stable complex could be a non-active one – carboxylates have always played …

Settore CHIM/03 - Chimica Generale E Inorganicafatty acids anti-tumor drugs organotin
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Dibuthyltin(IV) Complexes with Caffeic acid: Apoptotic Effect on human cancer cells

2013

Caffeic acidApoptosisDibuthyltin(IV)Dibuthyltin(IV); Caffeic acid; Apoptosis
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Carbocysteine degradation catalyzed by organotin(IV) compounds.

2008

Carbocysteine degradation organotin(IV) compoundsSettore CHIM/03 - Chimica Generale E Inorganica
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Novel metallic and organometallic based antiproliferative complexes: Integrated methodologies of evaluation

2005

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ATTIVITÀ CITOTOSSICA DEI COMPLESSI DIORGANOSTAGNO(IV)-N-ACETILCISTEINA SU CELLULE DI MELANOMA A-375.

2005

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Synthesis, structural investigation and biological activity of metal ions complexes of N-acetylcysteine and carbocysteine

2006

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Complessi di nuova sintesi di derivati della cisteina con ioni metallici

2006

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Synthesis and characterization of diorganotin(IV)complexes with Phenothiazine class Drugs. Biological and Theoretical studies on cytotoxic activity

2005

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Studi strutturali e indagini biologiche di nuovi complessi di rutenio(III) con 1- tioglucosio e 1-metiluracile

2006

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Computational studies of new metallic ions complexes of antioxidant dipeptides

2005

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Synthesis and characterization of some new ruthenium complexes with ligands of biological interest

2005

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Synthesis, structural investigation and biological activity of new diorganotin(IV) N-acetylcysteine Complexes.

2006

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Organometallic Complexes with Biological Molecules. Structural investigation of cis-diammineplatinum(II)-Porphyrin derivatives.

2009

cis-diammineplatinum(II) PorphyrinSettore CHIM/03 - Chimica Generale E Inorganica
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CCDC 830010: Experimental Crystal Structure Determination

2013

Related Article: Ornella Pellerito, Cristina Prinzivalli, Elisabetta Foresti, Piera Sabatino, Michele Abbate, Girolamo Casella, Tiziana Fiore, Michelangelo Scopelliti, Claudia Pellerito, Michela Giuliano, Giulia Grasso, Lorenzo Pellerito|2013|J.Inorg.Biochem.|125|16|doi:10.1016/j.jinorgbio.2013.04.008

Space GroupCrystallographyCrystal SystemCrystal StructureTriphenyl-((2-propylpentanoyl)oxy)-tinCell ParametersExperimental 3D Coordinates
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