Author: Martin Kotora

0000000000954322

AUTHOR

Martin Kotora

0000-0003-4491-7091

showing 8 related works from this author

Ir-Catalyzed Cycloaddition of Tribenzocyclyne with Biphenylenes

2021

We demonstrate that Ir-catalyzed C-C bond activation in biphenylenes followed by a reaction with tribenzocyclyne is a suitable method for synthesizing strained and unknown monoadducts with the tetradehydrotetrabenzo[a,c,e,i]cyclododecene scaffold ([12]annulenes). Modification of reaction conditions also furnished [12]annulene products with cis and/or trans double bonds formed by hydrogen transfer. The [9]annulene side product was formed upon the reaction of the benzyl radical with tribenzocyclyne during the Bergman cyclization. All isolated compounds were fully characterized by HRMS, NMR, and X-ray diffraction analysis.

Reaction conditionschemistry.chemical_classificationDouble bondchemistryBergman cyclizationOrganic ChemistrySide productHydrogen transferAnnuleneMedicinal chemistryCycloadditionCatalysisJournal of Organic Chemistry

researchProduct

CCDC 2074639: Experimental Crystal Structure Determination

2021

Related Article: Jaroslav Jacko, Monika Staś, Lubomír Rulíšek, Ivana Císařová, Martin Kotora|2022|J.Org.Chem.|87|744|doi:10.1021/acs.joc.1c01118

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates13-benzyldibenzo[34:89]indeno[1'2':67]cyclonona[12-l]phenanthrene benzene solvate

researchProduct

CCDC 2074638: Experimental Crystal Structure Determination

2021

Related Article: Jaroslav Jacko, Monika Staś, Lubomír Rulíšek, Ivana Císařová, Martin Kotora|2022|J.Org.Chem.|87|744|doi:10.1021/acs.joc.1c01118

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterstribenzo[acn]tetraphenyleneExperimental 3D Coordinates

researchProduct

CCDC 2074634: Experimental Crystal Structure Determination

2021

Related Article: Jaroslav Jacko, Monika Staś, Lubomír Rulíšek, Ivana Císařová, Martin Kotora|2022|J.Org.Chem.|87|744|doi:10.1021/acs.joc.1c01118

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters13141920-tetradehydrotribenzo[1112:34:78]cyclododeca[12-l]phenanthreneExperimental 3D Coordinates

researchProduct

CCDC 2074637: Experimental Crystal Structure Determination

2021

Related Article: Jaroslav Jacko, Monika Staś, Lubomír Rulíšek, Ivana Císařová, Martin Kotora|2022|J.Org.Chem.|87|744|doi:10.1021/acs.joc.1c01118

Space GroupCrystallography67-bis(trimethylsilyl)-13141920-tetradehydrobenzo[h]tribenzo[1112:34:78]cyclododeca[12-f]quinoline diethyl ether solvateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 2074635: Experimental Crystal Structure Determination

2021

Related Article: Jaroslav Jacko, Monika Staś, Lubomír Rulíšek, Ivana Císařová, Martin Kotora|2022|J.Org.Chem.|87|744|doi:10.1021/acs.joc.1c01118

Space GroupCrystallographyCrystal Systemtribenzo[1112:34:78]cyclododeca[12-l]phenanthrene benzene solvateCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 2074640: Experimental Crystal Structure Determination

2021

Related Article: Jaroslav Jacko, Monika Staś, Lubomír Rulíšek, Ivana Císařová, Martin Kotora|2022|J.Org.Chem.|87|744|doi:10.1021/acs.joc.1c01118

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates13-benzyldibenzo[34:89]indeno[1'2':67]cyclonona[12-l]phenanthrene benzene solvate

researchProduct

CCDC 2074636: Experimental Crystal Structure Determination

2021

Related Article: Jaroslav Jacko, Monika Staś, Lubomír Rulíšek, Ivana Císařová, Martin Kotora|2022|J.Org.Chem.|87|744|doi:10.1021/acs.joc.1c01118

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterstribenzo[1112:34:78]cyclododeca[12-l]phenanthrene benzene unknown solvateExperimental 3D Coordinates

researchProduct

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