0000000001085175
AUTHOR
Michael Lutter
Cis versus Trans: The Coordination Environment about the Tin(IV) Atom in Spirocyclic Amino Alcohol Derivatives.
The syntheses of amino alcohols MeN(CH2 CH2 CMe2 OH)2 (1), MeN(CMe2 CH2 OH)(CH2 CMe2 OH) (2), MeN(CH2 CH2 CH2 OH)(CH2 CMe2 OH) (3), MeN(CH2 CH2 CMe2 OH)(CH2 CMe2 OH) (4), MeN(CH2 CH2 CMe2 OH)(CH2 CH2 OH) (5), and MeN(CH2 CH2 OH) (CH2 CH2 CH2 OH) (6) as well as spirocyclic tin(IV) alkoxides spiro-[nBuN(CH2 CMe2 O)2 ]2 Sn (7), spiro-[MeN(CH2 CH2 CMe2 O)2 ]2 Sn (8), spiro-[para-FC6 H4 N (CH2 CMe2 O)2 ]2 Sn (9), spiro-[MeN(CMe2 CH2 O)(CH2 CMe2 O)]2 Sn (10), spiro-[MeN(CH2 CH2 CH2 O)(CH2 CMe2 O)]2 Sn (11), spiro-[MeN(CH2 CH2 CMe2 O)(CH2 CMe2 O)]2 Sn (12), spiro-[MeN(CH2 CH2 CMe2 O)(CH2 CH2 O)]2 Sn (13) and spiro-[MeN(CH2 CH2 O)(CH2 CH2 CH2 O)]2 Sn (14) are reported. The compounds were characteri…
Novel Stannatrane N(CH2CMe2O)2(CMe2CH2O)SnO-t-Bu and Related Oligonuclear Tin(IV) Oxoclusters. Two Isomers in One Crystal
The syntheses of the alkanolamine N(CH2CMe2OH)2(CMe2CH2OH) (1), of the stannatrane N(CH2CMe2O)2(CMe2CH2O)SnO-t-Bu (2), and of the trinuclear tin oxocluster 3 consisting of the two isomers [(μ3-O)(O-t-Bu){Sn(OCH2CMe2)(OCMe2CH2)2N}3] (3a) and [(μ3-O)(μ3-O-t-Bu){Sn(OCH2CMe2)(OCMe2CH2)2N}3] (3b) as well as the isolation of a few crystals of the hexanuclear tin oxocluster [LSnOSn(OH)3LSnOH]2 [L = N(CH2CMe2O)2(CMe2CH2O)] (4) are reported. The compounds were characterized by 1H, 13C, 15N, and 119Sn (1–3) nuclear magnetic resonance and infrared spectroscopy, electrospray ionization mass spectrometry, and single-crystal X-ray diffraction analysis (1–4). A graph set analysis was performed for compoun…
CCDC 1483889: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Michael Lutter, Dieter Schollmeyer, Wolf Hiller, and Klaus Jurkschat|2016|Inorg.Chem.|55|10218|doi:10.1021/acs.inorgchem.6b01429
CCDC 1858288: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1858294: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1483890: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Michael Lutter, Dieter Schollmeyer, Wolf Hiller, and Klaus Jurkschat|2016|Inorg.Chem.|55|10218|doi:10.1021/acs.inorgchem.6b01429
CCDC 1858297: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1483888: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Michael Lutter, Dieter Schollmeyer, Wolf Hiller, and Klaus Jurkschat|2016|Inorg.Chem.|55|10218|doi:10.1021/acs.inorgchem.6b01429
CCDC 1496144: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Michael Lutter, Dieter Schollmeyer, Wolf Hiller, and Klaus Jurkschat|2016|Inorg.Chem.|55|10218|doi:10.1021/acs.inorgchem.6b01429
CCDC 1858291: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1858296: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1858292: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1858290: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1858293: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1858295: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952
CCDC 1858289: Experimental Crystal Structure Determination
Related Article: Britta Glowacki, Roman Pallach, Michael Lutter, Fabian Roesler, Hazem Alnasr, Dieter Schollmeyer, Cederic Thomas, Klaus Jurkschat|2018|Chem.-Eur.J.|24|19266|doi:10.1002/chem.201803952