Author: Sarah Molinari

0000000001098080

AUTHOR

Sarah Molinari

Influence of Outer-Sphere Anions on the Photoluminescence from Samarium(II) Crown Complexes.

Three samarium(II) crown ether complexes, [Sm(15-crown-5)2]I2 (1), [Sm(15-crown-5)2]I2·CH3CN (2), and [Sm(benzo-15-crown-5)2]I2 (3), have been prepared via the reaction of SmI2 with the corresponding crown ether in either THF or acetonitrile in good to moderate yields. The compounds have been characterized by single crystal X-ray diffraction and a variety of spectroscopic techniques. In all cases, the Sm(II) centers are sandwiched between two crown ether molecules and are bound by the five etheric oxygen atoms from each crown ether to yield 10-coordinate environments. Despite the higher symmetry crystal class of 1 (R3c), the samarium center resides on a general position, whereas in 2 and 3 …

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CCDC 2088521: Experimental Crystal Structure Determination

Related Article: Todd N. Poe, Sarah Molinari, Maria J. Beltran-Leiva, Cristian Celis-Barros, Harry Ramanantoanina, Thomas E. Albrecht-Scho��nzart|2021|Inorg.Chem.|60|15196|doi:10.1021/acs.inorgchem.1c01606

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CCDC 2086032: Experimental Crystal Structure Determination

Related Article: Todd N. Poe, Sarah Molinari, Maria J. Beltran-Leiva, Cristian Celis-Barros, Harry Ramanantoanina, Thomas E. Albrecht-Scho��nzart|2021|Inorg.Chem.|60|15196|doi:10.1021/acs.inorgchem.1c01606

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CCDC 2088520: Experimental Crystal Structure Determination

Related Article: Todd N. Poe, Sarah Molinari, Maria J. Beltran-Leiva, Cristian Celis-Barros, Harry Ramanantoanina, Thomas E. Albrecht-Scho��nzart|2021|Inorg.Chem.|60|15196|doi:10.1021/acs.inorgchem.1c01606

research product

CCDC 2086030: Experimental Crystal Structure Determination

Related Article: Todd N. Poe, Sarah Molinari, Maria J. Beltran-Leiva, Cristian Celis-Barros, Harry Ramanantoanina, Thomas E. Albrecht-Scho��nzart|2021|Inorg.Chem.|60|15196|doi:10.1021/acs.inorgchem.1c01606

research product

CCDC 2088522: Experimental Crystal Structure Determination

Related Article: Todd N. Poe, Sarah Molinari, Maria J. Beltran-Leiva, Cristian Celis-Barros, Harry Ramanantoanina, Thomas E. Albrecht-Scho��nzart|2021|Inorg.Chem.|60|15196|doi:10.1021/acs.inorgchem.1c01606

research product

CCDC 2086031: Experimental Crystal Structure Determination

Related Article: Todd N. Poe, Sarah Molinari, Maria J. Beltran-Leiva, Cristian Celis-Barros, Harry Ramanantoanina, Thomas E. Albrecht-Scho��nzart|2021|Inorg.Chem.|60|15196|doi:10.1021/acs.inorgchem.1c01606

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PEPhysical Sciences and Engineering
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