0000000001172910

AUTHOR

Corinne Rondeau-mouro

showing 2 related works from this author

Identification and quantification of phosphorus in cheeses - methodological investigations by solid-state 31P NMR spectroscopy

2008

International audience; NMR has been shown to be an interesting tool for investigating dairy foods, in particular cheese products, for which the method is non-destructive and well suited for investigating their compounds showing different structure and mobility during ripening. Solid-state magic angle spinning 31P NMR spectroscopy was used to characterize the structure and composition of semi-hard cheeses. Assignment including overlapping resonances from mobile/immobile phosphorylated serine residues and inorganic calcium phosphates, has been realised using different NMR techniques (spin echo, cross polarisation and single pulse excitation) and by comparison with spectra of literature. Stud…

PHOSPHORUSSPECTROSCOPYCHEESE[SPI.GPROC] Engineering Sciences [physics]/Chemical and Process Engineering[SDV.IDA]Life Sciences [q-bio]/Food engineering[SPI.GPROC]Engineering Sciences [physics]/Chemical and Process Engineering[SDV.IDA] Life Sciences [q-bio]/Food engineeringSOLID-STATE 31P NMR
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Distribution and mobility of phosphates and sodium ions in cheese by solid-state 31 P and double-quantum filtered 23 Na NMR spectroscopy

2010

The feasibility of solid-state magic angle spinning (MAS) (31)P nuclear magnetic resonance (NMR) spectroscopy and (23)Na NMR spectroscopy to investigate both phosphates and Na(+) ions distribution in semi-hard cheeses in a non-destructive way was studied. Two semi-hard cheeses of known composition were made with two different salt contents. (31)P Single-pulse excitation and cross-polarization MAS experiments allowed, for the first time, the identification and quantification of soluble and insoluble phosphates in the cheeses. The presence of a relatively 'mobile' fraction of colloidal phosphates was evidenced. The detection by (23)Na single-quantum NMR experiments of all the sodium ions in t…

chemistry.chemical_classificationIon exchangeSodium0402 animal and dairy scienceAnalytical chemistrychemistry.chemical_elementSalt (chemistry)04 agricultural and veterinary sciencesGeneral ChemistryNuclear magnetic resonance spectroscopy040401 food science040201 dairy & animal scienceIonColloid0404 agricultural biotechnologychemistryMagic angle spinningGeneral Materials ScienceSpectroscopyMagnetic Resonance in Chemistry
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