Author: J. Valkonen

0000000001298772

AUTHOR

J. Valkonen

Influence of sample pan on the thermal behaviour of KSCN measured with TG

Abstract In this study, the influence of the sample pan on the thermal behaviour of potassium thiocyanate (KSCN) was investigated. The measurements were performed with thermogravimetry (TG) and the two sample pans used were a platinum pan and a ceramic crucible. The samples were heated to 400–950 °C and the thermal products were identified by powder diffraction. The thermal behaviour of KSCN was found to be dependent on the sample pan used. With the platinum sample pan KSCN reacted in the first step into a mixture of K 2 SO 4 and potassium tetracyanoplatinate (K 2 Pt(CN) 4 ). In the second step, the mixture reacted further to pure K 2 SO 4 . In the ceramic sample crucible, however, the reac…

0000000001298772

AUTHOR

J. Valkonen

Influence of sample pan on the thermal behaviour of KSCN measured with TG

Use of kinetic DTA and TG methods for compatibility tests on 2,4,6--trinitrotoluene

Effect of the crystallization on the phase transitions IV ⇐ III and IV ⇐ II of ammonium nitrate

Differential scanning calorimetric and Raman studies of phase transition V ⇌ IV of ammonium nitrate

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