0000000001299876

AUTHOR

M. Haukka

showing 95 related works from this author

One-Pot Synthesis, X-ray Single Crystal and Molecular Insight of Enaminone-Based β-Morpholino-/N-Methylpiperazinyl-/Pyrrolidinylpropiophenone

2020

One-pot synthesis of three enaminones, (E)-1-(4-chlorophenyl)-3-morpholinoprop-2-en-1-one 1, (E)-1-(4-chlorophenyl)-3-(4-methylpiperazin-1-yl)prop-2-en-1-one 2, and (E)-1-(4-chlorophenyl)-3-(pyrrolidin-1-yl)prop-2-en-1-one 3 were achieved. The synthetic protocol via three components reaction of p-chloroacetophenone with DMFDMA (N,N-dimethylformamid-dimethylacetal) and the corresponding secondary amines (morpholine/N-methylpiperazine/pyrrolidine) in dioxane under heating for 2.5–4 h at 102 °C yielded the requisite enaminones. This protocol has the advantage of no separation of intermediate, no need for column purification with quantitative yield for the target compounds. The chemical feature…

kemiallinen synteesiamiinitpyrrolidinemorpholineDMFDMAHirshfeld analysisβ-enaminoneN-methylpiperazineorgaaniset yhdisteetröntgenkristallografia
researchProduct

CCDC 1034603: Experimental Crystal Structure Determination

2015

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Space GroupCrystallographyCrystal SystemCrystal Structure[(Benzothiazole-2(3H)-thione)iodobromide]Cell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1528782: Experimental Crystal Structure Determination

2017

Related Article: M. K. Hossain, M. Haukka, R. Sillanpää, D. A. Hrovat, M. G. Richmond, E. Nordlander, A. Lehtonen|2017|Dalton Trans.|46|7051|doi:10.1039/C7DT00846E

24-di-t-butyl-6-{[(2-hydroxy-2-phenylethyl)amino]methyl}phenolSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1034601: Experimental Crystal Structure Determination

2015

Related Article: L. Koskinen, P. Hirva, A. Hasu, S. Jääskeläinen, J. Koivistoinen, M. Pettersson, M. Haukka|2015|CrystEngComm|17|2718|doi:10.1039/C4CE02449D

[(N-Methylbenzothiazole-2-thione)iodobromide]Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 872002: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal Structure(mu~2~-11'-dipropyl-1H1'H-22'-biimidazole)-tetracarbonyl-(dichloro)-di-rhodiumCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 637411: Experimental Crystal Structure Determination

2007

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Space GroupCrystallographyCrystal Systemcatena-((mu~2~-cis-bis(35-Dimethyl-1H-pyrazol-4-yl)selenide)-dichloro-mercury(ii) dimethylsulfoxide solvate)Crystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 637417: Experimental Crystal Structure Determination

2007

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Space GroupCrystallographycatena-(bis(mu~2~-cis-bis(35-Dimethyl-1H-pyrazolyl)selenide)-tetrakis(mu~2~-cyano)-dicyano-tri-cadmium(ii) methanol solvate)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 984540: Experimental Crystal Structure Determination

2014

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersbis(22'-(iodoniumdiyldisulfanediyl)bis(45-dihydro-1H-imidazol-3-ium)) iodide triiodideExperimental 3D Coordinates
researchProduct

CCDC 886205: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographycatena-((mu~2~-Aqua)-(mu~2~-22'-(13-phenylenebis(carbonylimino))-diacetato)-diaqua-copper dihydrate)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 840685: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterstetrakis(mu~2~-11'-Dibenzyl-22'-bi-imidazole)-tetra-aqua-tetra-silver tetranitrateExperimental 3D Coordinates
researchProduct

CCDC 1537189: Experimental Crystal Structure Determination

2017

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersdicarbonyl-chloro-(4'-chloro-22':6'2''-terpyridine)-ruthenium(ii) tricarbonyl-trichloro-ruthenium(ii)Experimental 3D Coordinates
researchProduct

CCDC 773478: Experimental Crystal Structure Determination

2011

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersbis(5-phenyl-1H-pyrazol-4-yl) selenide (5-phenyl-1H-pyrazol-4-yl) (3-phenyl-1H-pyrazol-4-yl) selenide ethanol solvateExperimental 3D Coordinates
researchProduct

CCDC 881316: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureTetrachloro-(N-(4-nitrophenyl)propanimidamide)-propanenitrile-platinum(iv)Cell ParametersExperimental 3D Coordinates
researchProduct

CCDC 881314: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterstetrachloro-(N-(3-nitrophenyl)propanimidamide)-(propiononitrile)-platinum(iv)Experimental 3D Coordinates
researchProduct

CCDC 957339: Experimental Crystal Structure Determination

2014

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Space GroupCrystallographyCrystal Systemdiiodo-bis(3-methyl-13-benzothiazole-2(3H)-thione)-di-goldCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 637413: Experimental Crystal Structure Determination

2007

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Space GroupCrystallographyCrystal Systemcatena-(bis(mu~2~-cis-bis(35-Dimethyl-1H-pyrazol-4-yl)selenide)-(mu~2~-trans-bis(35-dimethyl-1H-pyrazol-4-yl)selenide)-tetrachloro-di-copper(ii) dimethylsulfoxide solvate dihydrate)Crystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 902349: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal Structure1-(2-(4-Methylphenyl)-2-oxoethyl)pyridinium 1-[(2E)-3-amino-1-(4-methylphenyl)-1-oxobut-2-en-2-yl]pyridiniodecaborane butylpropanoateCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 881319: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyTetrachloro-(methyl propanimidoate)-(N-(3-nitrophenyl)propanimidamide)-platinum(iv)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 637412: Experimental Crystal Structure Determination

2007

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Space GroupCrystallographyCrystal Systemcatena-((mu~2~-trans-bis(35-dimethyl-1H-pyrazol-4-yl)selenide)-bis(mu~2~-thiocyanato)-bis(thiocyanato)-di-mercury(ii))Crystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 871907: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-[(110-Phenanthroline)-tetracarbonyl-dichloro-di-rhodium]Experimental 3D Coordinates
researchProduct

CCDC 1537327: Experimental Crystal Structure Determination

2017

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Space GroupCrystallographydichloro-bis(N-(22-dimethyl-34-dihydro-2H-pyrrol-5-yl)acetamide)-palladium(ii) dihydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 881315: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemTetrachloro-bis(N-(3-nitrophenyl)propanimidamide)-platinum(iv)Crystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 637416: Experimental Crystal Structure Determination

2007

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Space GroupCrystallographycatena-(bis(mu~2~-cis-bis(35-Dimethyl-1H-pyrazol-4-yl)selenide)-bis(mu~2~-thiocyanato)-cadmium(ii))Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 299923: Experimental Crystal Structure Determination

2011

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersbis(3-methyl-5-phenyl-1H-pyrazol-2-ium-4-yl) selenide sulfate monohydrateExperimental 3D Coordinates
researchProduct

CCDC 886203: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinatescatena-((mu~4~-2'-(13-Phenylenebis(carbonylimino))diacetato)-triaqua-strontium dihydrate)
researchProduct

CCDC 956724: Experimental Crystal Structure Determination

2013

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2-(35-Dimethyl-1H-pyrazol-1-yl)-2-(hydroxyimino)-N'-(1-(pyridin-2-yl)ethylidene)acetohydrazideSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 968918: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal Systembis(Hydroxyammonium) hexachloro-platinum(iv) 18-crown-6 solvateCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 886204: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-((mu2-22'-(13-phenylenebis(carbonylimino))diacetato)-tetra-aqua(hydroxy)-manganese(ii) dihydrate)Experimental 3D Coordinates
researchProduct

CCDC 872003: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal Structure(mu~2~-11'-dipropyl-1H1'H-22'-biimidazole)-tetracarbonyl-(dichloro)-di-rhodiumCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 914261: Experimental Crystal Structure Determination

2013

Related Article: S.Tomyn, M.Haukka, R.Nedelkov|2012|Acta Crystallogr.,Sect.E:Struct.Rep.Online|68|m1568|doi:10.1107/S160053681204826X

Space GroupCrystallographyCrystal SystemDiammine-(N-[2-(hydroxyimino)propionyl]-N'-[2-(oxidoimino)propionyl]propane-13-diamido)-iron(iii)Crystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 881311: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyTetrachloro-bis(propanenitrile)-platinum(iv)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 886200: Experimental Crystal Structure Determination

2013

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22'-(13-Phenylenebis(carbonylimino))diacetic acidSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1434350: Experimental Crystal Structure Determination

2015

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1-(1lambda5-Borinin-1-yl)-26-dimethyl-1lambda5-pyridineSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 299921: Experimental Crystal Structure Determination

2011

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Space GroupCrystallographybis(3-(2-pyridinio)-5-methyl-1H-pyrazol-4-yl) selenide dinitrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 881313: Experimental Crystal Structure Determination

2013

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Tetrachloro-bis(3-nitroaniline)-platinum(iv) dihydrateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 637415: Experimental Crystal Structure Determination

2007

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Space GroupCrystallographycatena-(bis(mu~2~-trans-bis(35-Dimethyl-1H-pyrazol-4-yl)selenide)-zinc(ii) dinitrate)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 2120378: Experimental Crystal Structure Determination

2021

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Space GroupCrystallographyCrystal SystemCrystal Structurecatena-[bis(mu-22'-[135-oxadiazinane-35-diylbis(azanidediyl)]bis(oxoacetato))-(mu-aqua)-bis(aqua)-tetra-potassium-di-nickel(ii)]Cell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1034600: Experimental Crystal Structure Determination

2015

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Space GroupCrystallographyCrystal System[(N-methylbenzothiazole-2-thione)ICl]Crystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1893862: Experimental Crystal Structure Determination

2019

Related Article: K. Znovjyak, I.O. Fritsky, I.A. Golenya, T.Y. Sliva, M. Haukka|2019|Acta Crystallogr.,Sect.E:Cryst.Commun.|75|358|doi:10.1107/S2056989019001531

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters{2-({[1-(2-methoxyethyl)-1H-imidazol-2-yl]methylidene}amino)-NN-bis[2-({[1-(2-methoxyethyl)-1H-imidazol-2-yl]methylidene}amino)ethyl]ethan-1-amine}-iron(ii) dihexafluorophosphateExperimental 3D Coordinates
researchProduct

CCDC 840686: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterstetrakis(mu~2~-11'-Dibenzyl-22'-bi-imidazole)-tetrakis(nitrato-O)-tetra-silver dichloromethane solvate dihydrateExperimental 3D Coordinates
researchProduct

CCDC 886206: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographycatena-((mu2-22'-(13-phenylenebis(carbonylimino))diacetato)-tri-aqua-zinc(ii) dihydrate)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1528783: Experimental Crystal Structure Determination

2017

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(24-di-t-butyl-6-({[2-oxido-2-phenylethyl]amino}methyl)phenolato)-(dimethyl sulfoxide)-dioxo-molybdenum(vi) unknown solvateExperimental 3D Coordinates
researchProduct

CCDC 886201: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemHexa-aqua-magnesium 22'-(13-phenylenebis(carbonylimino))diacetate hydrateCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 299922: Experimental Crystal Structure Determination

2011

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Space GroupCrystallographyCrystal Systembis(35-dimethyl-1H-pyrazol-4-yl) selenide monohydrateCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 871906: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal Systemcatena-[(22'-Bipyridine)-tetracarbonyl-dichloro-di-rhodium]Crystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 718361: Experimental Crystal Structure Determination

2010

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Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinateshexakis(mu~2~-eta^2^-ferrocenylethynyl)-tris(mu~2~-14-bis(diphenylphosphino)benzene)-di-copper-hexa-gold bis(hexafluorophosphate) acetone n-hexane solvate
researchProduct

CCDC 978372: Experimental Crystal Structure Determination

2014

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5-imino-34-diphenyl-15-dihydro-2H-pyrrol-2-oneSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 939036: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D CoordinatesPyridinium dipyridine-tetrakis(thiocyanato)-iron(iii)
researchProduct

CCDC 872001: Experimental Crystal Structure Determination

2013

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Space GroupCrystallographyCrystal SystemCrystal Structure(mu~2~-11'-dipropyl-1H1'H-22'-biimidazole)-tetracarbonyl-(dichloro)-di-rhodiumCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 796685: Experimental Crystal Structure Determination

2011

Related Article: M.Tuikka, M.Niskanen, P.Hirva, K.Rissanen, A.Valkonen, M.Haukka|2011|Chem.Commun.|47|3427|doi:10.1039/c0cc05726f

Space GroupCrystallography(22'-Bipyridine-44'-dicarboxylic acid-NN')-dicarbonyl-bis(iodo)-ruthenium bis(diiodine) methanol solvateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1034602: Experimental Crystal Structure Determination

2015

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Space GroupCrystallographyCrystal SystemCrystal Structure[(Benzothiazole-2(3H)-thione)iodochloride]Cell ParametersExperimental 3D Coordinates
researchProduct

CCDC 299920: Experimental Crystal Structure Determination

2011

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tris(1H-pyrazol-4-yl)selenonium ethylseleniteSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 637414: Experimental Crystal Structure Determination

2007

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Space GroupCrystallographycatena-(bis(mu2-cis-bis(35-Dimethyl-1H-pyrazol-4-yl)selenide)-aqua-copper(ii) dibromide monohydrate)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1026710: Experimental Crystal Structure Determination

2014

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2017

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2014

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2014

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2017

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2014

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2014

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2017

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2017

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2013

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2014

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2013

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