Author: Sandrine Ruchaud

0000000001301441

AUTHOR

Sandrine Ruchaud

showing 3 related works from this author

A combined experimental and theoretical study of the thermal [3+2] cycloaddition of carbonyl ylides with activated alkenes

2018

International audience; 4-Benzoyl-3,5-diaryltetrahydrofuran-2,2-dicarbonitriles were first synthesized from 2,2-dicyano-3-aryloxiranes and chalcones at toluene reflux; the 4,5-cis products proved to be predominantly formed and were isolated. Whereas shortened reaction times were observed by using microwave irradiation or catalytic cuprous chloride, no significant stereoselectivity change was in general noticed. Reacting 2,2-dicyano-3-aryloxiranes with 2-cyclopentenone next afforded 3-aryl-4-oxohexahydro-1H-cyclopenta[c]furan-1,1-dicarbonitriles, and the endo stereoisomers were isolated. That no stereoselectivity change was noticed in the presence of cuprous chloride rather suggests an impac…

Epoxide010402 general chemistryenones01 natural sciencesMedicinal chemistryAnalytical ChemistryCatalysisInorganic Chemistrychemistry.chemical_compound[SDV.SP.MED]Life Sciences [q-bio]/Pharmaceutical sciences/MedicationCascade reaction[3+2] cycloadditionEnamines[CHIM]Chemical SciencesTetrahydrofuransSpectroscopytheoretical calculationschemistry.chemical_classification[CHIM.ORGA]Chemical Sciences/Organic chemistry010405 organic chemistryOrganic ChemistryRegioselectivityCycloaddition0104 chemical sciencescarbonyl ylideschemistryYlide[SDV.MP.VIR]Life Sciences [q-bio]/Microbiology and Parasitology/VirologyStereoselectivityCis–trans isomerismJournal of Molecular Structure

researchProduct

CCDC 688220: Experimental Crystal Structure Determination

2017

Related Article: Samira Hamza-Reguig, Ghenia Bentabed-Ababsa, Luis R. Domingo, Mar Ríos-Gutiérrez, Stéphanie Philippot, Stéphane Fontanay, Raphaël E. Duval, Sandrine Ruchaud, Stéphane Bach, Thierry Roisnel, Florence Mongin|2018|J.Mol.Struct.|1157|276|doi:10.1016/j.molstruc.2017.12.052

Space GroupCrystallography4-benzoyl-5-(4-methoxyphenyl)-3-phenyldihydrofuran-22(3H)-dicarbonitrileCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 688217: Experimental Crystal Structure Determination

2017

Related Article: Samira Hamza-Reguig, Ghenia Bentabed-Ababsa, Luis R. Domingo, Mar Ríos-Gutiérrez, Stéphanie Philippot, Stéphane Fontanay, Raphaël E. Duval, Sandrine Ruchaud, Stéphane Bach, Thierry Roisnel, Florence Mongin|2018|J.Mol.Struct.|1157|276|doi:10.1016/j.molstruc.2017.12.052

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters4-oxo-3-phenylhexahydro-1H-cyclopenta[c]furan-11-dicarbonitrileExperimental 3D Coordinates

researchProduct

PEPhysical Sciences and Engineering
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