0000000001301756
AUTHOR
P.j. Van Koningsbruggen
Mossbauer spectroscopic study of the thermal spin crossover in [Fe(II)(isoxazole)(6)](ClO(4))(2)
The (57)Fe Mossbauer spectroscopy of mononuclear [Fe(II)(isoxazole)(6)](ClO(4))(2) has been studied to reveal the thermal spin crossover of Fe(II) between low-spin (S = 0) and high-spin (S = 2) states.Temperature-dependent spin transition curves have been constructed with the least-square fitted data obtained from the Mossbauer spectra measured at various temperatures between 84 and 270 K during a cooling and heating cycle. This compound exhibits an unusual temperature-dependent spin transition behaviour with T(C)(down arrow) = 223 and T(C)(up arrow) = 213 K occurring in the reverse order in comparison to those observed in SQUID observation and many other spin transition compounds. The comp…
CCDC 140484: Experimental Crystal Structure Determination
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CCDC 181860: Experimental Crystal Structure Determination
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CCDC 159367: Experimental Crystal Structure Determination
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CCDC 229670: Experimental Crystal Structure Determination
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CCDC 229675: Experimental Crystal Structure Determination
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CCDC 145000: Experimental Crystal Structure Determination
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CCDC 229674: Experimental Crystal Structure Determination
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CCDC 145001: Experimental Crystal Structure Determination
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CCDC 181859: Experimental Crystal Structure Determination
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CCDC 229671: Experimental Crystal Structure Determination
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CCDC 229676: Experimental Crystal Structure Determination
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CCDC 181857: Experimental Crystal Structure Determination
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CCDC 140485: Experimental Crystal Structure Determination
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CCDC 229669: Experimental Crystal Structure Determination
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CCDC 229673: Experimental Crystal Structure Determination
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CCDC 229672: Experimental Crystal Structure Determination
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CCDC 161006: Experimental Crystal Structure Determination
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CCDC 181858: Experimental Crystal Structure Determination
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CCDC 181861: Experimental Crystal Structure Determination
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CCDC 229677: Experimental Crystal Structure Determination
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CCDC 116040: Experimental Crystal Structure Determination
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