Author: Jesus M. Ugalde

0000000001301983

AUTHOR

Jesus M. Ugalde

showing 3 related works from this author

Enantiospecific Response in Cross-Polarization Solid-State Nuclear Magnetic Resonance of Optically Active Metal Organic Frameworks.

2020

We report herein on a NMR-based enantiospecific response for a family of optically active metal-organic frameworks. Cross-polarization of the 1H-13C couple was performed, and the intensities of the 13C nuclei NMR signals were measured to be different for the two enantiomers. In a direct-pulse experiment, which prevents cross-polarization, the intensity difference of the 13C NMR signals of the two nanostructured enantiomers vanished. This result is due to changes of the nuclear spin relaxation times due to the electron spin spatial asymmetry induced by chemical bond polarization involving a chiral center. These experiments put forward on firm ground that the chiral-induced spin selectivity e…

Magnetic Resonance SpectroscopyOptical Phenomenamedia_common.quotation_subject010402 general chemistry01 natural sciencesBiochemistryAsymmetryCatalysisColloid and Surface ChemistryPolarization (electrochemistry)Spin (physics)QuantumMetal-Organic Frameworksmedia_commonChemistryCircular DichroismRelaxation (NMR)General ChemistryCarbon-13 NMRMetal Organic FrameworkNMR0104 chemical sciencesChemical bondSolid-state nuclear magnetic resonanceChemical physicsSettore CHIM/03 - Chimica Generale E InorganicaCondensed Matter::Strongly Correlated ElectronsJournal of the American Chemical Society

researchProduct

CCDC 1990183: Experimental Crystal Structure Determination

2020

Related Article: Eider San Sebastian, Javier Cepeda, Uxua Huizi-Rayo, Alessio Terenzi, Daniel Finkelstein-Shapiro, Daniel Padro, Jose Ignacio Santos, Jon M. Matxain, Jesus M. Ugalde, Vladimiro Mujica|2020|J.Am.Chem.Soc.|142|17989|doi:10.1021/jacs.0c04537

Space GroupCrystallographycatena-[tris(mu-D-tartrato)-diaqua-di-yttrium(iii) trihydrate]Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 1990182: Experimental Crystal Structure Determination

2020

Related Article: Eider San Sebastian, Javier Cepeda, Uxua Huizi-Rayo, Alessio Terenzi, Daniel Finkelstein-Shapiro, Daniel Padro, Jose Ignacio Santos, Jon M. Matxain, Jesus M. Ugalde, Vladimiro Mujica|2020|J.Am.Chem.Soc.|142|17989|doi:10.1021/jacs.0c04537

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-[tris(mu-L-tartrato)-diaqua-di-yttrium(iii) tetrahydrate]Experimental 3D Coordinates

researchProduct

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