0000000001302163

AUTHOR

J. Latorre

showing 25 related works from this author

Formation of Pyrazol-1,3,4-Thiadiazoles through 1,3-Dipolar Cycloadditions of 3-Thioxo-[1,2,4]-Triazepin-5-one with Nitrilimines: An Experimental and…

2009

In this work the results of experimental and computational study of the title compounds and some ancillary compounds are reported. Two bicyclic pyrazol-1,3,4-thiadiazole derivatives were synthesized by reaction between 6-dimethylaminomethylene-3-thioxo-[1,2,4]- triazepin-5-one 1 and several nitrilimines 2a-f to give corresponding spirocycloadducts 3a-f, which undergo a rapid rearrangement leading to the new bicyclic compounds, 4a-f and 5a-f. These obtained bicyclic products were characterized by 1H and 13C NMR spectroscopy and finally by X-ray crystallography. Theoretical calculations have been carried out using DFT methods to rationalize the formation of the two new bicyclic compounds. Two…

Bicyclic moleculeStereochemistryChemistryOrganic ChemistryAncillary compoundsRegioselectivityCarbon-13 NMRRing (chemistry)Cleavage (embryo)CycloadditionCatalysisThiadiazolesComputational chemistryPhysical and Theoretical Chemistry
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CCDC 658959: Experimental Crystal Structure Determination

2007

Related Article: B.Verdejo, A.Ferrer, S.Blasco, C.E.Castillo, J.Gonzalez, J.Latorre, M.A.Manez, M.G.Basallote, C.Soriano, E.Garcia-Espana|2007|Inorg.Chem.|46|5707|doi:10.1021/ic700643n

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(6-(2-Aminoethyl)-36915-tetra-azabicyclo(9.3.1)pentadeca-1(15)1113-triene)-copper(ii) diperchlorate hemihydrateExperimental 3D Coordinates
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CCDC 209937: Experimental Crystal Structure Determination

2003

Related Article: M.Chadim, P.Diaz, E.Garcia-Espana, J.Hodacova, P.C.Junk, J.Latorre, J.M.Llinares, C.Soriano, J.Zavada|2003|New J.Chem.|27|1132|doi:10.1039/b303470d

Space GroupCrystallographyCrystal System310-Diazonia-613-diaza-1(12)-benzenacyclotetradecaphane bis(246-trinitrophenolate) acetone solvateCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 804809: Experimental Crystal Structure Determination

2012

Related Article: F.Reviriego, P.Navarro, V.J.Aran, M.L.Jimeno, E.Garcia-Espana, J.Latorre, M.J.R.Yunta|2011|J.Org.Chem.|76|8223|doi:10.1021/jo2012835

Space GroupCrystallographyCrystal System619-Dibutyl-391622-tetraoxa-61213192526-hexaazatricyclo[22.2.1.1^1114^]octacosa-1(27)1114(28)24-tetraene-2101523-tetrone hemihydrateCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 658957: Experimental Crystal Structure Determination

2007

Related Article: B.Verdejo, A.Ferrer, S.Blasco, C.E.Castillo, J.Gonzalez, J.Latorre, M.A.Manez, M.G.Basallote, C.Soriano, E.Garcia-Espana|2007|Inorg.Chem.|46|5707|doi:10.1021/ic700643n

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates(6-(2-(Naphthylmethyamino)ethyl)-36915-tetra-azabicyclo(9.3.1)pentadeca-1(15)1113-triene)-copper(ii) perchlorate
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CCDC 174510: Experimental Crystal Structure Determination

2002

Related Article: F.Escarti, C.Miranda, L.Lamarque, J.Latorre, E.Garcia-Espana, M.Kumar, V.J.Aran, P.Navarro|2002|Chem.Commun.||936|doi:10.1039/b110409h

Space GroupCrystallographyCrystal Systembis(mu4-111(35)-Dipyrazola-391319-tetra-azacycloicosaphane)-diaqua-bis(perchlorato-O)-tetra-copper(ii) diperchlorate dihydrateCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 652238: Experimental Crystal Structure Determination

2007

Related Article: M.Ruiz, R.Ortiz, L.Perello, J.Latorre, J.Server-Carrio|1997|J.Inorg.Biochem.|65|87|doi:10.1016/S0162-0134(96)00092-X

bis(Cinoxacinato)-bis(dimethylsulfoxide)-nickel(ii) tetrahydrateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 658956: Experimental Crystal Structure Determination

2007

Related Article: B.Verdejo, A.Ferrer, S.Blasco, C.E.Castillo, J.Gonzalez, J.Latorre, M.A.Manez, M.G.Basallote, C.Soriano, E.Garcia-Espana|2007|Inorg.Chem.|46|5707|doi:10.1021/ic700643n

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters6-(2-(Naphthylmethyammonio)ethyl)-615-diaza-39-diazoniabicyclo(9.3.1)pentadeca-1(15)1113-triene tris(dihydrogenphosphate) monohydrateExperimental 3D Coordinates
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CCDC 194482: Experimental Crystal Structure Determination

2003

Related Article: P.Diaz, M.G.Basallote, M.A.Manez, E.Garcia-Espana, L.Gil, J.Latorre, C.Soriano, B.Verdejo, S.V.Luis|2003|Dalton Trans.||1186|doi:10.1039/b209013a

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(2691216-Penta-aza(17)(26)pyridinophane)-copper(ii) diperchlorateExperimental 3D Coordinates
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CCDC 652237: Experimental Crystal Structure Determination

2007

Related Article: M.Ruiz, R.Ortiz, L.Perello, J.Latorre, J.Server-Carrio|1997|J.Inorg.Biochem.|65|87|doi:10.1016/S0162-0134(96)00092-X

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D CoordinatesAqua-bis(cinoxacinato)-copper(ii) trihydrate
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CCDC 730787: Experimental Crystal Structure Determination

2010

Related Article: F.Reviriego, A.Sanz, P.Navarro, J.Latorre, E.Garcia-Espana, M.Liu-Gonzalez|2009|Org.Biomol.Chem.|7|3212|doi:10.1039/b911053d

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersHomoveratrylammonium 35-bis(ethoxycarbonyl)pyrazolateExperimental 3D Coordinates
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CCDC 730786: Experimental Crystal Structure Determination

2010

Related Article: F.Reviriego, A.Sanz, P.Navarro, J.Latorre, E.Garcia-Espana, M.Liu-Gonzalez|2009|Org.Biomol.Chem.|7|3212|doi:10.1039/b911053d

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersbeta-Phenethylammonium 35-bis(ethoxycarbonyl)pyrazolateExperimental 3D Coordinates
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CCDC 209938: Experimental Crystal Structure Determination

2003

Related Article: M.Chadim, P.Diaz, E.Garcia-Espana, J.Hodacova, P.C.Junk, J.Latorre, J.M.Llinares, C.Soriano, J.Zavada|2003|New J.Chem.|27|1132|doi:10.1039/b303470d

Space GroupCrystallographyCrystal Systemcatena-(trans-IIII-RRSS-(mu~2~-Chloro)-(361013-tetraaza-1(12)-benzenacyclotetradecaphane)-copper(ii) perchlorate)Crystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 804808: Experimental Crystal Structure Determination

2012

Related Article: F.Reviriego, P.Navarro, V.J.Aran, M.L.Jimeno, E.Garcia-Espana, J.Latorre, M.J.R.Yunta|2011|J.Org.Chem.|76|8223|doi:10.1021/jo2012835

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters619-dimethyl-391622-tetraoxa-61213192526-hexaazatricyclo[22.2.1.1^1114^]octacosa-1(27)1114(28)24-tetraene-2101523-tetrone acetonitrile solvateExperimental 3D Coordinates
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CCDC 209939: Experimental Crystal Structure Determination

2003

Related Article: M.Chadim, P.Diaz, E.Garcia-Espana, J.Hodacova, P.C.Junk, J.Latorre, J.M.Llinares, C.Soriano, J.Zavada|2003|New J.Chem.|27|1132|doi:10.1039/b303470d

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterstrans-IIII-RRSS-Chloro-(361013-tetraaza-1(12)-benzenacyclotetradecaphane)-zinc(ii) chloride monohydrateExperimental 3D Coordinates
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CCDC 658958: Experimental Crystal Structure Determination

2007

Related Article: B.Verdejo, A.Ferrer, S.Blasco, C.E.Castillo, J.Gonzalez, J.Latorre, M.A.Manez, M.G.Basallote, C.Soriano, E.Garcia-Espana|2007|Inorg.Chem.|46|5707|doi:10.1021/ic700643n

6-(2-(Naphthylmethyamino)ethyl)-6915-triaza-3-azoniabicyclo(9.3.1)pentadeca-1(15)1113-triene perchlorate monohydrateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 220976: Experimental Crystal Structure Determination

2004

Related Article: E.Garcia-Espana, P.Gavina, J.Latorre, C.Soriano, B.verdejo|2004|J.Am.Chem.Soc.|126|5082|doi:10.1021/ja039577h

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(mu~2~-Carbonato)-(mu~2~-81619223035-hexaaza-1226-diazonia-tetracyclo(26.2.2.2^710^.1^26^)pentatriaconta-1(30)2(35)3579283133-nonaenato)-aqua-diperchlorato-di-copper(ii) diperchlorate hydrateExperimental 3D Coordinates
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CCDC 649152: Experimental Crystal Structure Determination

2008

Related Article: B.Verdejo, S.Blasco, E.Garcia-Espana, F.Lloret, P.Gavina, C.Soriano, S.Tatay, H.R.Jimenez, A.Domenech, J.Latorre|2007|Dalton Trans.||4726|doi:10.1039/b708186c

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates(mu~2~-13(25)-dipyridina-2(26)-pyridina-59121519-pentaazacycloicosaphane)-(mu~2~-imidazol-1-yl-NN')-aqua-bromo-di-copper(ii) bis(trifluoromethanesulfonate) trihydrate
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CCDC 119069: Experimental Crystal Structure Determination

1999

Related Article: M.A.Bernardo, F.Pina, B.Escuder, E.Garcia-Espana, M.L.Godino-Salido, J.Latorre, S.V.Luis, J.A.Ramirez, C.Soriano|1999|J.Chem.Soc.,Dalton Trans.||915|doi:10.1039/a808649d

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(N-(3-Aminopropyl)-N'-3-(anthracen-9-ylmethyl)aminopropylethane-12-diamino)-chloro-copper(ii) chloride monohydrateExperimental 3D Coordinates
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CCDC 240641: Experimental Crystal Structure Determination

2005

Related Article: C.Miranda, F.Escarti, L.Lamarque, E.Garcia-Espana, P.Navarro, J.Latorre, F.Lloret, H.R.Jimenez, M.J.R.Yunta|2005|Eur.J.Inorg.Chem.||189|doi:10.1002/ejic.200400671

Space GroupCrystallography(mu~2~-3711151923-Hexa-aza-113(35)-dipyrazolacyclotetracosaphane)-di-copper(ii) diperchlorateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 240640: Experimental Crystal Structure Determination

2005

Related Article: C.Miranda, F.Escarti, L.Lamarque, E.Garcia-Espana, P.Navarro, J.Latorre, F.Lloret, H.R.Jimenez, M.J.R.Yunta|2005|Eur.J.Inorg.Chem.||189|doi:10.1002/ejic.200400671

(mu~2~-369131619-Hexa-aza-111(35)-dipyrazolacycloicosaphane)-di-zinc(ii) diperchlorateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 810034: Experimental Crystal Structure Determination

2011

Related Article: M.P.Clares, S.Blasco, M.Inclan, L.del C.Agudo, B.Verdejo, C.Soriano, A.Domenech, J.Latorre, E.Garcia-Espana|2011|Chem.Commun.|47|5988|doi:10.1039/c1cc10526d

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersAqua-(N-(quinolin-4-ylmethyl)-2-(36915-tetra-azabicyclo[9.3.1]pentadeca-1(15)1113-trien-6-yl)ethanamine)-manganese(ii) diperchlorateExperimental 3D Coordinates
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CCDC 240642: Experimental Crystal Structure Determination

2005

Related Article: C.Miranda, F.Escarti, L.Lamarque, E.Garcia-Espana, P.Navarro, J.Latorre, F.Lloret, H.R.Jimenez, M.J.R.Yunta|2005|Eur.J.Inorg.Chem.||189|doi:10.1002/ejic.200400671

Space GroupCrystallographyCrystal SystemCrystal Structure(mu2-3711151923-Hexa-aza-113(35)-dipyrazolacyclotetracosaphane)-di-zinc(ii) diperchlorateCell ParametersExperimental 3D Coordinates
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CCDC 220975: Experimental Crystal Structure Determination

2004

Related Article: E.Garcia-Espana, P.Gavina, J.Latorre, C.Soriano, B.verdejo|2004|J.Am.Chem.Soc.|126|5082|doi:10.1021/ja039577h

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersAqua-(19-carboxylato-81619223035-hexaaza-1226-diazonia-tetracyclo(26.2.2.2^710^.1^26^)pentatriaconta-1(30)2(35)3579283133-nonaenato)-copper(ii) triperchlorate dihydrateExperimental 3D Coordinates
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CCDC 810035: Experimental Crystal Structure Determination

2011

Related Article: M.P.Clares, S.Blasco, M.Inclan, L.del C.Agudo, B.Verdejo, C.Soriano, A.Domenech, J.Latorre, E.Garcia-Espana|2011|Chem.Commun.|47|5988|doi:10.1039/c1cc10526d

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates(N-((Quinolin-2-yl)methyl)-2-(36915-tetra-azabicyclo[9.3.1]pentadeca-1(15)1113-trien-6-yl)-ethanamine)-manganese(ii) diperchlorate monohydrate
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