0000000001302193
AUTHOR
Abdullah Saleh Alamary
X-ray Crystal Structure and Hirshfeld Analysis of Gem-Aminals-Based Morpholine, Pyrrolidine, and Piperidine Moieties
The gem-aminals of 1,2-dimorpholinoethane (1) and 1-morpholino-3-morpholinium bromide propane (2) were synthesized by reaction of two molar ratio of morpholine with the halogenating agents in the presence of basic condition (K2CO3) in acetone at room temperature (RT) overnight. The structures of the centro-symmetric compound 1 and the morpholinium salt derivative 2 were assigned unambiguous by single crystal X-ray diffraction analysis and compared with the 1,2-di(pyrrolidin-1-yl)ethane 3 and 1,2-di(piperidin-1-yl)ethane 4. The 1,2-dimorpholinoethane molecule has a center of symmetry at the midpoint of the C-C bond of the ethyl moiety leading to two equivalent halves. It crystallized in mono…
Synthesis of Enaminones-Based Benzo[d]imidazole Scaffold: Characterization and Molecular Insight Structure
(E)-1-(1H-Benzo[d]imidazol-2-yl)-3-(dimethylamino)prop-2-en-1-one 2 was synthesized by one-pot synthesis protocol of 2-acetyl benzo[d]imidazole with dimethylformamide dimethylacetal (DMF-DMA) in xylene at 140 °
CCDC 2039255: Experimental Crystal Structure Determination
Related Article: Abdullah Mohammed Al-Majid, Matti Haukka, Saied M. Soliman, Abdullah Saleh Alamary, Saeed Alshahrani, M. Ali, Mohammad Shahidul Islam, Assem Barakat|2021|Symmetry|13|20|doi:10.3390/sym13010020
CCDC 1999582: Experimental Crystal Structure Determination
Related Article: Saeed Alshahrani, Saied M. Soliman, Abdullah Saleh Alamary, Abdullah Mohammed Al-Majid, Matti Haukka, Sammer Yousuf, Assem Barakat|2020|Crystals|10|955|doi:10.3390/cryst10100955
CCDC 2022360: Experimental Crystal Structure Determination
Related Article: Abdullah Mohammed Al-Majid, Matti Haukka, Saied M. Soliman, Abdullah Saleh Alamary, Saeed Alshahrani, M. Ali, Mohammad Shahidul Islam, Assem Barakat|2021|Symmetry|13|20|doi:10.3390/sym13010020
CCDC 2032100: Experimental Crystal Structure Determination
Related Article: Saeed Alshahrani, Saied M. Soliman, Abdullah Saleh Alamary, Abdullah Mohammed Al-Majid, Matti Haukka, Sammer Yousuf, Assem Barakat|2020|Crystals|10|955|doi:10.3390/cryst10100955