Author: Constantinos C. Stoumpos

0000000001303990

AUTHOR

Constantinos C. Stoumpos

From Bowls to Capsules: Assembly of Hexanuclear Ni II Rings Tailored by Alkali Cations

An anionic hexanuclear NiII metallamacrocycle with endo and exo linking sites has been employed as a building block to generate a series of capsules and bowls of nanometric size. The supramolecular arrangement of the {Ni6 } rings was tailored by the size of the alkali cations, showing the transition from {Ni6 -M2 -Ni6 } capsules (M=LiI and NaI ) to {Ni6 -M} bowls (M=KI and CsI ). The alkyl co-cations are determinant to stabilize the assemblies by means of CH⋅⋅⋅π interactions on the exo side of the metallamacrocycles. The effect on the topology of the supramolecular assemblies of the cation size, cation charge, Et3 NH+ or Me4 N+ counter cations has been analyzed. Magnetic measurements reveal…

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Cover Feature: From Bowls to Capsules: Assembly of Hexanuclear Ni II Rings Tailored by Alkali Cations (Chem. Eur. J. 49/2020)

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CCDC 1996425: Experimental Crystal Structure Determination

Related Article: Júlia Mayans, Constantinos C. Stoumpos, Mercé Font-Bardia, Albert Escuer|2020|Chem.-Eur.J.|26|11158|doi:10.1002/chem.202001900

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CCDC 1996430: Experimental Crystal Structure Determination

Related Article: Júlia Mayans, Constantinos C. Stoumpos, Mercé Font-Bardia, Albert Escuer|2020|Chem.-Eur.J.|26|11158|doi:10.1002/chem.202001900

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CCDC 1996426: Experimental Crystal Structure Determination

Related Article: Júlia Mayans, Constantinos C. Stoumpos, Mercé Font-Bardia, Albert Escuer|2020|Chem.-Eur.J.|26|11158|doi:10.1002/chem.202001900

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CCDC 1996428: Experimental Crystal Structure Determination

Related Article: Júlia Mayans, Constantinos C. Stoumpos, Mercé Font-Bardia, Albert Escuer|2020|Chem.-Eur.J.|26|11158|doi:10.1002/chem.202001900

research product

CCDC 1996427: Experimental Crystal Structure Determination

Related Article: Júlia Mayans, Constantinos C. Stoumpos, Mercé Font-Bardia, Albert Escuer|2020|Chem.-Eur.J.|26|11158|doi:10.1002/chem.202001900

research product

CCDC 1996429: Experimental Crystal Structure Determination

Related Article: Júlia Mayans, Constantinos C. Stoumpos, Mercé Font-Bardia, Albert Escuer|2020|Chem.-Eur.J.|26|11158|doi:10.1002/chem.202001900

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PEPhysical Sciences and Engineering
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