Author: Bassam Abu Thaher

0000000001308599

AUTHOR

Bassam Abu Thaher

Crystal structures of pure 3-(4-bromo-2-chlorophenyl)-1-(pyridin-4-yl)benzo[4,5]imidazo[1,2-d][1,2,4]triazin-4(3H)-one and contaminated with 3-(4-bromophenyl)-1-(pyridin-4-yl)benzo[4,5]imidazo[1,2-d][1,2,4]triazin-4(3H)-one

The side product of the cyclocondensation reaction between ethyl benzimidazole-2-carboxylate and the nitrile imine of the corresponding hydrazonyl chloride, C20H11BrClN5O, crystallized in two crystal forms. Form (1) is a co-crystal of the target compound (without any chlorine substituent) and a side product containing a Cl atom in position 2 of the bromophenyl group, C20H12BrN5O·0.143C20H11BrClN5O. (2) contains the pure side product. The slightly different conformation of the ring systems leads to a different packing of (1) and (2), but both crystal structures are dominated by p-p interactions.

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CSD 2099609: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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CSD 2099612: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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CSD 2099610: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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CCDC 2049251: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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CCDC 2042388: Experimental Crystal Structure Determination

Related Article: Saeb Aliwaini, Bassam Abu Thaher, Ihab Al-Masri, Nabil Shurrab, Said El-Kurdi, Dieter Schollmeyer, Basem Qeshta, Mariam Ghunaim, Ren�� Csuk, Stefan Laufer, Lars Kaiser, Hans-Peter Deigner|2021|Molecules|26|4065|doi:10.3390/molecules26134065

research product

CCDC 2049252: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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CSD 2099611: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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