Author: Oliver Riester

0000000001308602

AUTHOR

Oliver Riester

Efficient Synthesis and X-ray Structure of [1,2,4]Triazolo[4,3-a]pyridines via Oxidative Cyclization Using N-Chlorosuccinimide (NCS)

Triazolopyridines are a family of compounds that, owing to their biological activity, have many pharmaceutical applications. In this study, 3-(pyridine-4-yl)-[1,2,4]triazolo[4,3-a]pyridine and 6-bromo-3-(pyridine-4-yl)-[1,2,4]triazolo[4,3-a]pyridine were synthesized by using the chlorinated agent NCS for hydrazones under very mild conditions. The characterization of these compounds was achieved by 1H NMR, 13C NMR, FTIR, MS and X-ray diffraction. The compound 3-(pyridine-4-yl)-[1,2,4]triazolo[4,3-a]pyridine was crystallized in the monoclinic space group P 21/c with a = 15.1413(12), b = 6.9179(4), c = 13.0938(8) Å, β = 105.102(6)°, V = 1324.16(16)Å3, Z = 4, and R = 0.0337. Also compound 6-bro…

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CSD 2099609: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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CSD 2099612: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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CSD 2099610: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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CCDC 2049251: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

research product

CCDC 2049252: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

research product

CSD 2099611: Experimental Crystal Structure Determination

Related Article: Said El-Kurdi, Bassam Abu Thaher, Kanan Wahedy, Dieter Schollmeyer, Levin Nopper, Oliver Riester, Hans-Peter Deigner|2021|Crystals|11|1156|doi:10.3390/cryst11101156

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PEPhysical Sciences and Engineering
- PE2Fundamental Constituents of Matter
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LSLife Sciences
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