Author: Johannes J. Mayer

0000000001308786

AUTHOR

Johannes J. Mayer

showing 3 related works from this author

Synthesis of copper(II) and gold(III) bis(NHC)-pincer complexes

2016

Abstract CuII and AuIII chlorido complexes bearing the bis(NHC) carbazolide pincer ligand (bimca) were synthesized by transmetallation from the respective lithium complex [Li(bimca)] (NHC=N-heterocyclic carbene). In the case of copper, two different molecular structures were obtained depending on the copper source. With Cu(II) chloride the paramagnetic mononuclear [Cu(bimca)Cl] complex is formed and has been characterized by EPR spectroscopy and X-ray structure analysis, while copper(I) chloride leads under oxidation to a dinuclear structure in which two cationic [CuII(bimca)] moieties are bridged by one chlorido ligand. The positive charge is compensated by the [CuCl2]− counter ion, as pro…

010405 organic chemistryChemistryLigandCationic polymerizationchemistry.chemical_elementGeneral Chemistry010402 general chemistry01 natural sciencesCopperMedicinal chemistry0104 chemical sciencesPincer movementlaw.inventionchemistry.chemical_compoundTransmetalationlawElectron paramagnetic resonancePincer ligandCarbeneZeitschrift für Naturforschung B

researchProduct

CCDC 1492154: Experimental Crystal Structure Determination

2016

Related Article: Eva Jürgens, Oliver Back, Johannes J. Mayer, Katja Heinze, Doris Kunz|2016|Z.Naturforsch.,B:Chem.Sci.|71|1011|doi:10.1515/znb-2016-0158

Space GroupCrystallographyCrystal SystemCrystal Structure(mu-chloro)-bis(36-di-t-butyl-18-bis(3-methyl-23-dihydro-1H-imidazol-1-ylidene)-9H-carbazole)-di-copper(ii) dichloro-copper(i) tetrahydrofuran solvateCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 1492153: Experimental Crystal Structure Determination

2016

Related Article: Eva Jürgens, Oliver Back, Johannes J. Mayer, Katja Heinze, Doris Kunz|2016|Z.Naturforsch.,B:Chem.Sci.|71|1011|doi:10.1515/znb-2016-0158

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(36-di-t-butyl-18-bis(3-methyl-23-dihydro-1H-imidazol-1-ylidene)-9H-carbazole)-chloro-copper(ii) acetonitrile solvateExperimental 3D Coordinates

researchProduct

PEPhysical Sciences and Engineering
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