Author: Adedamola A. Opalade

0000000001309424

AUTHOR

Adedamola A. Opalade

showing 7 related works from this author

New Route to Polynuclear Ni(II) and Cu(II) Complexes with Bridging Oxime Groups That Are Inaccessible by Conventional Preparations

2019

A series of new polynuclear complexes of divalent Ni and Cu with 2-cyano-2-oximino-acetic acid (later AACO2-) were obtained as the result of the ligand modification reaction in the process of complexation, using 2-cyano-2-oximino-acetates such as methyl- (later as MeCO), and ethyl- (as ECO later on). Synthesized compounds were characterized by spectroscopic methods, thermal analysis, magnetochemistry, and X-ray crystallography. Crystal data revealed the formation of the dimeric [Ni(AACO)(H2O)3]2·H2O (1), trimeric K2[Ni3(AACO)4(H2O)4]·4H2O (2), and K2[Cu3(AACO)4(H2O)4]·4H2O (3) complexes, with bridging NO-groups cyanoxime dianions. In the latter two compounds, the AACO2– anions adopt cis-arr…

chemistry.chemical_classification010405 organic chemistryGeneral Chemistry010402 general chemistryCondensed Matter PhysicsOxime01 natural sciencesAntiferromagnetic coupling0104 chemical sciencesDivalentMetalchemistry.chemical_compoundCrystallographychemistryMagnetochemistryvisual_artCrystal datavisual_art.visual_art_mediumGeneral Materials ScienceThermal analysisCrystal Growth & Design

researchProduct

CCDC 1473520: Experimental Crystal Structure Determination

2019

Related Article: Adedamola A. Opalade, Carlos J. Gomez-Garcia, Nikolay Gerasimchuk|2019|Cryst.Growth Des.|19|678|doi:10.1021/acs.cgd.8b01262

Space GroupCrystallographybis(mu-cyano((hydroxy)imino)acetato)-hexaaqua-di-nickel(ii) dihydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

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CCDC 1473522: Experimental Crystal Structure Determination

2019

Related Article: Adedamola A. Opalade, Carlos J. Gomez-Garcia, Nikolay Gerasimchuk|2019|Cryst.Growth Des.|19|678|doi:10.1021/acs.cgd.8b01262

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinatesoxalamide

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CCDC 1473516: Experimental Crystal Structure Determination

2019

Related Article: Adedamola A. Opalade, Carlos J. Gomez-Garcia, Nikolay Gerasimchuk|2019|Cryst.Growth Des.|19|678|doi:10.1021/acs.cgd.8b01262

Space GroupCrystallographyethyl cyano(hydroxyimino)acetateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 1473523: Experimental Crystal Structure Determination

2019

Related Article: Adedamola A. Opalade, Carlos J. Gomez-Garcia, Nikolay Gerasimchuk|2019|Cryst.Growth Des.|19|678|doi:10.1021/acs.cgd.8b01262

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-[tris(mu-aqua)-bis(mu-cyano(oxidoimino)acetato)-copper-di-potassium]Experimental 3D Coordinates

researchProduct

CCDC 1473518: Experimental Crystal Structure Determination

2019

Related Article: Adedamola A. Opalade, Carlos J. Gomez-Garcia, Nikolay Gerasimchuk|2019|Cryst.Growth Des.|19|678|doi:10.1021/acs.cgd.8b01262

Space GroupCrystallographycatena-[bis(mu-aqua)-tetrakis(mu-cyano(oxidoimino)acetato)-hexaaqua-tri-copper-di-potassium]Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 1473524: Experimental Crystal Structure Determination

2019

Related Article: Adedamola A. Opalade, Carlos J. Gomez-Garcia, Nikolay Gerasimchuk|2019|Cryst.Growth Des.|19|678|doi:10.1021/acs.cgd.8b01262

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-[bis(mu-aqua)-tetrakis(mu-cyano(oxidoimino)acetato)-hexaaqua-tri-nickel-di-potassium]Experimental 3D Coordinates

researchProduct

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