Author: N. Srinivasan

0000000001313808

AUTHOR

N. Srinivasan

showing 3 related works from this author

Crystal structure of thecisandtranspolymorphs of bis[μ-2-(1,3-benzothiazol-2-yl)phenolato]-κ3N,O:O;κ3O:N,O-bis[fac-tricarbonylrhenium(I)]

2017

The title dinuclear complex, [Re2(C13H8NOS)2(CO)6], crystallizes in two polymorphs where the 2-(1,3-benzothiazol-2-yl)phenolate ligands and two carbonyl groups aretrans- (I) orcis-arranged (II) with respect to the [Re2O2(CO)4] core. PolymorphsIandIIexhibit a crystallographically imposed centre of symmetry and a twofold rotation axis, respectively. The structures may be described as being formed by two octahedrally distorted metal-coordinating units fused through μ-oxido bridges, leading to edge-sharing dimers. The crystal packing is governed by C—H...O hydrogen-bonding interactions, forming chains parallel to thecaxis inIand a three-dimensional network inII.

crystal structureStereochemistrychemistry.chemical_elementGeneral ChemistryCrystal structureRhenium010402 general chemistry010403 inorganic & nuclear chemistryCondensed Matter Physics01 natural sciencespolymorphism0104 chemical sciencesrhenium tricarbonyl complexeslcsh:ChemistryCrystallographylcsh:QD1-999Polymorphism (materials science)chemistryGeneral Materials ScienceCis–trans isomerismActa Crystallographica Section E Crystallographic Communications

researchProduct

CCDC 1529700: Experimental Crystal Structure Determination

2017

Related Article: M. Priyatharsini, B. Shankar, M. Sathiyendiran, N. Srinivasan, R.V. Krishnakumar|2017|Acta Crystallogr.,Sect.E:Cryst.Commun.|73|310|doi:10.1107/S2056989017001347

Space GroupCrystallographyCrystal Systemtrans-bis{mu-2-(13-benzothiazol-2-yl)phenolato}-hexacarbonyl-di-rhenium(i)Crystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 1529701: Experimental Crystal Structure Determination

2017

Related Article: M. Priyatharsini, B. Shankar, M. Sathiyendiran, N. Srinivasan, R.V. Krishnakumar|2017|Acta Crystallogr.,Sect.E:Cryst.Commun.|73|310|doi:10.1107/S2056989017001347

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscis-bis{mu-2-(13-benzothiazol-2-yl)phenolato}-hexacarbonyl-di-rhenium(i)Experimental 3D Coordinates

researchProduct

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