Author: Jonas Rein

0000000001316513

AUTHOR

Jonas Rein

showing 2 related works from this author

Electrochemical C−H Functionalization of (Hetero)Arenes—Optimized by DoE

2020

Abstract A novel approach towards the activation of different arenes and purines including caffeine and theophylline is presented. The simple, safe and scalable electrochemical synthesis of 1,1,1,3,3,3‐hexafluoroisopropanol (HFIP) aryl ethers was conducted using an easy electrolysis setup with boron‐doped diamond (BDD) electrodes. Good yields up to 59 % were achieved. Triethylamine was used as a base as it forms a highly conductive media with HFIP, making additional supporting electrolytes superfluous. The synthesis was optimized using Design of Experiment (DoE) techniques giving a detailed insight to the significance of the reaction parameters. The mechanism was investigated by cyclic volt…

boron-doped diamond540 Chemistry and allied sciencesanodeElectrolyte010402 general chemistryElectrochemistry01 natural sciencesCatalysislaw.inventionC−H functionalizationchemistry.chemical_compoundlawelectrolysisElectrochemistryTriethylaminecaffeineElectrolysis010405 organic chemistryCommunicationArylOrganic ChemistryGeneral ChemistryCombinatorial chemistryCommunications0104 chemical scienceschemistry540 ChemieElectrodeSurface modificationCyclic voltammetryChemistry – A European Journal

researchProduct

CCDC 1988067: Experimental Crystal Structure Determination

2020

Related Article: Maurice Dörr, Johannes L. Röckl, Jonas Rein, Dieter Schollmeyer, Siegfried R. Waldvogel|2020|Chem.-Eur.J.|26|10195|doi:10.1002/chem.202001171

8-[(111333-hexafluoropropan-2-yl)oxy]-137-trimethyl-37-dihydro-1H-purine-26-dioneSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

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PEPhysical Sciences and Engineering
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