Author: Yury Brusentsev

0000000001322779

AUTHOR

Yury Brusentsev

showing 2 related works from this author

Synthesis of Sterically Hindered Chiral 1,4-Diols from Different Lignan-Based Backbones

2013

Methods for synthetic modifications of the natural dibenzylbutyrolactone lignan hydroxymatairesinol into chiral 1,4-diols with different lignan-derived backbones have been developed. A stepwise procedure, involving alkylation and oxidation, was shown to be successful and several highly substituted 1,4-diols were prepared. Some substituted butyrolactones resisted alkylation and led to the formation unusually stable hemiketals (butyrolactols). The formation of stable hemiketals was investigated in detail, showing that different backbone structures influence the formation and reactivity of the hemiketals.

Steric effectsLignanchemistry.chemical_compoundHydroxymatairesinolchemistryOrganic ChemistryOrganic chemistryReactivity (chemistry)AlkylationSynlett

researchProduct

CCDC 973751: Experimental Crystal Structure Determination

2013

Related Article: Yury Brusentsev, Mikko M. Hänninen, Patrik Eklund|2013|Synlett|24|2423|doi:10.1055/s-0033-1340084

Space GroupCrystallographyCrystal System22'-(817-Dimethoxy-1015-dioxatricyclo[14.2.2.2^69^]docosa-1(18)68161921-hexaene-34-diyl)dipropan-2-olCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

PEPhysical Sciences and Engineering
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LSLife Sciences
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