Environmentally friendly ionic liquids – (2-Hydroxyethyl)ammonium carboxylates

6533b7d7fe1ef96bd126955c

RESEARCH PRODUCT

Environmentally friendly ionic liquids – (2-Hydroxyethyl)ammonium carboxylates

Sanita Pavloviča

subject

Chemistry Ķīmija ķīmijas tehnoloģijas un biotehnoloģija Ķīmija

description

VIDEI DRAUDZĪGIE JONU ŠĶIDRUMI, (2-HIDROKSIETIL)AMONIJA KARBOKSILĀTI, AKŪTAIS TOKSISKUMS, ĶĪMISKĀ NOĀRDĪŠANĀS, BIOLOĢISKĀ NOĀRDĪŠANĀS, KNĒVENĀGELA KONDENSĀCIJAS REAKCIJAS, KUMARĪNU ATVASINĀJUMI, HANČA ESTERIS Darbā sintezēti (2-hidroksietil)amonija karboksilāti – formiāti, acetāti un laktāti. Pētītie jonu škidrumi (JŠ) kvalitatīvi raksturoti ar 1H KMR un kvantitatīvi ar AEŠH/MS, elementanalīzi un potenciometrisko titrēšanu neūdens vidē. JŠ ar fizikāli-ķīmiskām metodēm ir noteikts – ūdens saturs, termiskā stabilitāte, ūdens šķīdumu pH, polaritāte un ar bioloģiskām – akūtais toksiskums (letālās LC50 koncentrācijas), ķīmiskā un bioloģiskā noārdīšanās. JŠ vidēs ir veiktas karbonilsavienojumu kondensācijas reakcijas ar CH-skābēm un heterociklisko savienojumu – kumarīna atvasinājumu un Hanča estera sintēze bez papildus katalizatoru izmantošanas. Raksturotas un salīdzinātas dažādu veidu ietekmes uz reakcijas produktu veidošanās ātrumu un reģioselektivitāti – (2-hidroksietil)amonija rindas JŠ spēja sadarboties tandemā kā šķīdinātājam un katalizatoram, to ūdens šķīdumu pH vērtību jeb pseido-pH, kopējās polaritātes, JŠ katjona un anjona ietekmes.-

year	journal	country	edition	language
2014-01-01

https://dspace.lu.lv/dspace/handle/7/4028

PEPhysical Sciences and Engineering
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SHSocial Sciences and Humanities
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