6533b7dbfe1ef96bd1270140

RESEARCH PRODUCT

Crystal structure of 4,6-O-ethylidene-N-(2-hydroxybenzylidene)-β-D-glucopyranosylamine

Chebrolu P. RaoKari RissanenAjay K. SahPauli Saarenketo

subject

DiffractionGlucosamineMagnetic Resonance SpectroscopyAnomerSingle CrystalsMolecular StructureChemistryStereochemistryOrganic ChemistrySynthesis (Chemical)Saccharide MoietyH-1 Nmr StudiesGeneral MedicineCrystal structureBiochemistryAnalytical ChemistryCrystallographyX-Ray DiffractionLattice StructureProton NMRCrystal StructureMoietyCrystallization

description

4,6-O-Ethylidene-N-(2-hydroxybenzylidene)-β-D-glucopyranosylamine was synthesized and characterized using analytical, spectral and single-crystal X-ray diffraction methods. The anomeric nature of the saccharide moiety was proposed based on 1H NMR studies and was confirmed by the crystal structure. The lattice structure of this compound was compared with that of its analogues.

10.1016/s0008-6215(01)00284-1http://dspace.library.iitb.ac.in/xmlui/handle/10054/819