Mikrokalorimetra veiktspējas pārbaude un nitrocelulozes bāzētu vielu stabilitātes noteikšana un šo rezultātu salīdzinājums ar hromatogrāfijas rezultātiem

6533b7dbfe1ef96bd127041f

RESEARCH PRODUCT

Mikrokalorimetra veiktspējas pārbaude un nitrocelulozes bāzētu vielu stabilitātes noteikšana un šo rezultātu salīdzinājums ar hromatogrāfijas rezultātiem

Kaspars Meijers

subject

Etilcentralīts Mikrokalorimetrija Mikrokalorimetra veiktspēja STANAG Difenilamīns Ķīmija

description

Mikrokalorimetra veiktspējas pārbaude un nitrocelulozes bāzētu vielu stabilitātes noteikšana un šo rezultātu salīdzinājums ar hromatogrāfijas rezultātiem. Meijers K., zinātniskais vadītājs Dr. Chem., asoc. Prof. Mekšs P. maģistra darbs, 48 lappuses, 19 attēli, 13 tabulas, 39 literatūras avoti, 2 pielikumi. Latviešu valodā. Darbā ir veikta mikrokalorimetra veiktspējas pārbaude, kā arī nitrocelulozes bāzētu vielu stabilitātes izpēte, izmantojot mikrokalorimetru un AEŠH, kur kā stabilizators tiek izmantots difenilamīns un etilcentralīts. Mikrokalorimetra veiktspējas pārbaudei izmantota iekārtas iekšējā pārbaudes metode, kā arī pielietots bifenila tests. Nitrocelulozes bāzētu vielu mikrokalorimetriskā izpētē paraugi tika pētīti neizmainītā sastāvā, kā arī samalti speciālās manuālās viena valča dzirnavās, vai sagriezti, lai noteiktu to drošību un iespēju turpmākai pielietošanai un uzglabāšanai. Izvērtētas mikrokalorimetriskas siltumplūsmas līknes, kā arī veikts mikrokalorimetrisko un hromatogrāfiski iegūto datu salīdzinājums to turpmākai drošai uzglabāšanai, atbilstoši STANAG. Papildus tika veikts neliels gāzu hromatogrāfijas-masspektrometrijas eksperiments, lai identificētu iespējamās papildvielas paraugos.

year	journal	country	edition	language
2022-01-01

https://dspace.lu.lv/dspace/handle/7/59429

PEPhysical Sciences and Engineering
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SHSocial Sciences and Humanities
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