No biomasas iegūta levoglikozenona un tā degradācijas produktu noteikšana ātrās pirolīzes produktos, izmantojot UHPLC-UV-QDa sistēmu

6533b823fe1ef96bd127ef91

RESEARCH PRODUCT

No biomasas iegūta levoglikozenona un tā degradācijas produktu noteikšana ātrās pirolīzes produktos, izmantojot UHPLC-UV-QDa sistēmu

Daniela Godiņa

subject

STABILITĀTE LEVOGLIKOZENONS DEGRADĀCIJAS KINĒTIKA ULTRA AUGSTAS EFEKTIVITĀTES ŠĶIDRUMA HROMATOGRĀFIJA Ķīmija DERIVATIZĀCIJA

description

Literatūras apskatā apkopota informācija par levoglikozenona potenciālajām izmantošanas iespējām, tā izdalīšanas un noteikšanas metodēm, kā arī tā stabilitāti un iespējamajiem degradācijas produktiem. Apkopota informācija par savienojumu stabilitātes noteikšanas metodiku. Izmantojot UHPLC-UV sistēmu, izstrādāta metode levoglikozenona un tā degradācijas produktu identifikācijai, kā arī veikta metodes analītisko parametru noteikšana. Pēc izstrādātās UHPLC-UV metodes veikti levoglikozenona standartvielas un ātrās pirolīzes produktu – kondensātu un to ekstrakcijas frakciju – stabilitātes pētījumi dažādās šķīdinātāju sistēmās, divās temperatūrās un mainot šķīduma vides pH. Izmantojot UHPLC-MS sistēmu un veicot derivatizāciju ar 2,4-dinitrofenilhidrazīnu, izstrādāta metode levoglikozenona noteikšanai, kā arī veikta metodes analītisko parametru noteikšana.

year	journal	country	edition	language
2019-01-01

https://dspace.lu.lv/dspace/handle/7/46729

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