6533b826fe1ef96bd128462a

RESEARCH PRODUCT

Semipermeable membrane to retain platinum atoms in the electrodeposition process of alpha spectrometry sources

F. Vera ToméM.f. Da SilvaJ.c. SoaresJ.l. Ferrero CalabuigD. Juanes BarberC. Roldán GarcíaA. Martín Sánchez

subject

RadiationMaterials scienceAlpha spectrometryAnalytical chemistrychemistry.chemical_elementActinideRutherford backscattering spectrometryCathodelaw.inventionAnodechemistrylawScientific methodSemipermeable membranePlatinum

description

Abstract In earlier work alpha sources electrodeposited on stainless steel backings were analyzed by X-ray fluorescence (XRF) and Rutherford backscattering spectrometry (RBS) finding that during the electrodeposition process large quantities of platinum from the anode were deposited on the cathode surface jointly with the actinides. In the present work, a method to retain platinum atoms using an electrodeposition cell with a semipermeable membrane located between anode and cathode is proposed and tested. The XRF and RBS of alpha sources electrodeposited using this method show that there is less platinum on the stainless steel backing, thereby improving the quality of sources to be measured by alpha spectrometry.

https://doi.org/10.1016/s0969-8043(97)10057-4