6533b826fe1ef96bd1285068

RESEARCH PRODUCT

Assignment of1H and13C NMR data for (−)-methyl thyrsiflorin A and some scopadulan precursors

M. Luisa MarinRamón J. ZaragozáManuel ArnóMiguel A. González

subject

Nuclear magnetic resonanceChemistryNMR spectroscopy of stereoisomersProton NMRResonancePhysical chemistryGeneral Materials ScienceGeneral ChemistryFluorine-19 NMRCarbon-13 NMRDEPTSpectroscopyMethyl thyrsiflorin A

description

The 1H and 13C NMR spectral analysis of synthetic (−)-methylthyrsiflorin A and 10 scopadulan precursors is reported. Resonance assignments were based on one- and two-dimensional NMR techniques, which included 1H, 13C, DEPT and HMQC and also 1D NOE difference spectroscopy. Copyright © 2001 John Wiley & Sons, Ltd.

https://doi.org/10.1002/mrc.841