6533b827fe1ef96bd1286dad

RESEARCH PRODUCT

Chemical degradation products of lignin and humic substances part I Synthesis, structure verification and gas chromatographic separation of chlorinated vanillins and syringaldehydes

J. HyötyläinenJuha Knuutinen

subject

chemistry.chemical_classificationEnvironmental EngineeringChromatographyHealth Toxicology and MutagenesisPublic Health Environmental and Occupational HealthGeneral MedicineGeneral ChemistryMass spectrometryPollutionAldehydeCapillary gas chromatographychemistry.chemical_compoundChromatographic separationchemistryEnvironmental ChemistryOrganic chemistryLigninGas chromatographyChemical decomposition

description

Abstract Chlorinated vanillins (4-hydroxy-3-methoxybenzaldehydes) and syringaldehydes (3,5-dimethoxy-4-hydroxy-benzaldehydes) were synthesized and their purities and structures were examined by quartz capillary gas chromatography and mass spectrometry. The detailed procedures for the synthesis, gas chromatographic separation and mass spectroscopic features are presented.

https://doi.org/10.1016/0045-6535(93)90078-j