Fāžu pāreju kinētikas pētīšanas metožu salīdzinājums farmaceitiski aktīvu vielu polimorfu un solvātu veidotām sistēmām

6533b82afe1ef96bd128bbae

RESEARCH PRODUCT

Fāžu pāreju kinētikas pētīšanas metožu salīdzinājums farmaceitiski aktīvu vielu polimorfu un solvātu veidotām sistēmām

Agnese Dravniece

subject

description

Izvērtēta dažādu cietfāžu pārejas kinētikas pētīšanas metožu piemērotība atšķirīgām farmaceitiski aktīvo vielu kristālisko formu sistēmām. Lai izvērtētu katru no fāžu pārejas raksturošanas procesiem - eksperimentālos apstākļus, detektēšanas metodes un matemātisko rezultātu aprēķinus -, veikti polimorfo formu un solvātu cietfāžu pārejas kinētikas pētījumi. Pētītas antazolīna maleāta polimorfo formu pārejas A→C un B→C, antazolīna oksalāta solvāta desolvatācija B→C→A, bikarfēna hidrogēnhlorīda polimorfo formu pāreja A→B, solvāta desolvatācija X→B, hidrāta dehidratācija H→A un memantīna hidrogēnhlorīda dehidratācija H→A paaugstinātā temperatūrā. Parauga sastāva noteikšanai pētījuma laikā lietotas pulvera rentgendifraktometrijas un termogravimetrijas metodes, bet datu analīzei izvēlētas trīs kvantitatīvās analīzes metodes. Cietfāžu pārejas aprakstītas ar piemērotāko kinētikas modeli. Fāžu pārejas aktivācijas enerģijas aprēķināšanai lietotas gan modeļu piemērošanas, gan bezmodeļu metodes.

year	journal	country	edition	language
2014-01-01

https://dspace.lu.lv/dspace/handle/7/20906

PEPhysical Sciences and Engineering
- PE2Fundamental Constituents of Matter
  - PE2_1Theory of fundamental interactions
  - PE2_2 Phenomenology of fundamental interactions
  - PE2_3Experimental particle physics with accelerators
  - PE2_4Experimental particle physics without accelerators
  - PE2_6Nuclear, hadron and heavy ion physics
  - PE2_8Gas and plasma physics
  - PE2_5Classical and quantum physics of gravitational interactions
  - PE2_7Nuclear and particle astrophysics
  - PE2_9 Electromagnetism
  - PE2_10Atomic, molecular physics
  - PE2_11Ultra-cold atoms and molecules
  - PE2_18Equilibrium and non-equilibrium statistical mechanics: steady states and dynamics
  - PE2_14Lasers, ultra-short lasers and laser physics
  - PE2_17Metrology and measurement
  - PE2_16Non-linear physics
  - PE2_12Optics, non-linear optics and nano-optics
  - PE2_13Quantum optics and quantum information
  - PE2_15Thermodynamics
- PE1Mathematics
  - PE1_1Logic and foundations
  - PE1_6Geometry and global analysis
  - PE1_8Analysis
  - PE1_7Topology
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  - PE1_12Mathematical physics
  - PE1_11Theoretical aspects of partial differential equations
  - PE1_13Probability
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  - PE1_15Generic statistical methodology and modelling
  - PE1_4 Algebraic and complex geometry
  - PE1_19Scientific computing and data processing
  - PE1_2Algebra
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  - PE1_21Application of mathematics in sciences
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  - PE1_3Number theory
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- PE11Materials Engineering
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  - PE11_7Engineering of metal oxides
  - PE11_8Engineering of alternative established or emergent materials
  - PE11_9Nanomaterials engineering, e.g. nanoparticles, nanoporous materials, 1D & 2D nanomaterials
  - PE11_10Soft materials engineering, e.g. gels, foams, colloids
  - PE11_11Porous materials engineering, e.g. covalent-organic, metal-organic, porous aromatic frameworks
  - PE11_12Semi-conducting and magnetic materials engineering
  - PE11_13Metamaterials engineering
  - PE11_14Computational methods for materials engineering
LSLife Sciences
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  - LS1_14Innovative methods and modelling in molecular, structural and synthetic biology
  - LS1_10Synthetic biology
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  - LS1_9Molecular mechanisms of signalling processes
  - LS1_7Molecular biophysics, biomechanics, bioenergetics
- LS2Integrative Biology: from Genes and Genomes to Systems
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  - LS2_3Epigenetics
  - LS2_2Gene editing
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  - LS2_9Metabolomics
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  - LS4_1Organ and tissue physiology and pathophysiology
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- LS9Biotechnology and Biosystems Engineering
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SHSocial Sciences and Humanities
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