Metodes izstrāde un validācija pesticīdu atliekvielu noteikšanai Camellia sinensis lapās ar AEŠH-MS/MS un GH-MS/MS

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RESEARCH PRODUCT

Metodes izstrāde un validācija pesticīdu atliekvielu noteikšanai Camellia sinensis lapās ar AEŠH-MS/MS un GH-MS/MS

subject

CAMELLIA SINENSIS VALIDĀCIJA MASSPEKTROMETRIJA HROMATOGRĀFIJA PESTICĪDI Ķīmija

description

Metodes izstrāde un validācija pesticīdu atliekvielu noteikšanai Camellia sinensis lapās ar AEŠH-MS/MS un GH-MS/MS. Lankovska A., zinātniskās vadītājas Dr.chem. Pugajeva I., M.Sc., LU doktorante Ikkere L.E. Maģistra darbs, 40 lappuses, 17 attēli, 8 tabulas, 34 literatūras avoti, 6 pielikumi. Latviešu valodā. Darbā apkopota literatūra par tēju ķīmisko sastāvu, pesticīdu klasifikāciju, oficiālajām paraugu sagatavošanas metodēm, traucējošajiem efektiem pesticīdu noteikšanā un Eiropas Komisijas izdotajiem validācijas standartiem. Darbā veikta metodes validācija 121 savienojuma noteikšanai kaltētās Camellia Sinensis lapās ar augsti efektīvo šķidrumu hromatogrāfiju apvienojumā ar tandēma masspektrometrisko detektoru un 55 savienojumu detektēšanai, izmantojot gāzu hromatogrāfiju apvienojumā ar tandēma masspektrometrisko detektoru Iegūtie rezultāti izvērtēti atbilstoši SANTE/12682/2019 noteiktajiem validācijas kritērijiem. Metodes pielietojums pārbaudīts, analizējot komerciāli pieejamās tējas.

year	journal	country	edition	language
2021-01-01

https://dspace.lu.lv/dspace/handle/7/55109

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