6533b835fe1ef96bd129e950
RESEARCH PRODUCT
Synthesis and properties of magnetic iron oxide/platinum nanocomposites
Lidiya KulikovaAija KruminaVera SergaMikhail MaiorovDaniela Karashanovasubject
Materials scienceNanocompositeInorganic chemistryIron oxidechemistry.chemical_elementHematitechemistry.chemical_compoundchemistryvisual_artvisual_art.visual_art_mediumCarboxylateHexachloroplatinatePlatinumPyrolysisMagnetiteNuclear chemistrydescription
Iron oxide/platinum nanocomposites have been synthesized by the extractive-pyrolytic method (EPM) involving gradual decomposition of iron capronate and n-trioctylammonium hexachloroplatinate initially produced by solvent extraction. The content of platinum in the composites was 1.2 wt%, 2.4 wt% and 4.8 wt%. Phase composition, morphology and magnetic properties of the produced materials were investigated. XRD analysis and magnetic measurements show that the magnetic phase (magnetite Fe3O4) dominates in a carrier sample produced by the pyrolysis of iron carboxylate, but hematite α-Fe2O3 exists there as an admixture. Referring to the TEM results, the produced composites contain ultra-disperse platinum particles on the carrier, and the mean size of these varies from 3 nm to 9 nm.
| year | journal | country | edition | language |
|---|---|---|---|---|
| 2015-03-09 | IOP Conference Series: Materials Science and Engineering |