[1,2-Bis(diphenylphosphanyl)ethane-&#954;2P,P&#8242;]{2-[(4-nitrobenzoylmethyl)diphenylphosphanyl]phenyl-&#954;2C,C&#8242;}palladium(II) trifluoromethanesulfonate&#8211;dichloromethane&#8211;n-hexane (1/1/0.5)

6533b836fe1ef96bd12a0731

RESEARCH PRODUCT

[1,2-Bis(diphenylphosphanyl)ethane-&#954;2P,P&#8242;]{2-[(4-nitrobenzoylmethyl)diphenylphosphanyl]phenyl-&#954;2C,C&#8242;}palladium(II) trifluoromethanesulfonate&#8211;dichloromethane&#8211;n-hexane (1/1/0.5)

Corrado Rizzoli Kazem Karami Farzaneh Borzooie

subject

description

In the cation of the title compound, [Pd(C26H19NO3P)(C26H24P2)]CF3O3S&#183;CH2Cl2&#183;0.5C6H14, the PdII atom has a slightly tetrahedrally distorted square-planar coordination geometry. The PdC3P and PdC2P2 five-membered metallacycles adopt envelope and twist conformations, respectively. In the crystal, intermolecular C&#8212;H...O hydrogen bonds link cations and anions into a three-dimensional network. The dichloromethane solvent molecule is disordered over three orientations with a site-occupancy ratio of 0.5/0.3/0.2. The n-hexane solvent molecule has a crystallographically imposed centre of symmetry.

year	journal	country	edition	language
2011-04-01	Acta Crystallographica Section E

10.1107/s1600536811008075 http://scripts.iucr.org/cgi-bin/paper?S1600536811008075

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6533b836fe1ef96bd12a0731

RESEARCH PRODUCT

[1,2-Bis(diphenylphosphanyl)ethane-&amp;#954;2P,P&amp;#8242;]{2-[(4-nitrobenzoylmethyl)diphenylphosphanyl]phenyl-&amp;#954;2C,C&amp;#8242;}palladium(II) trifluoromethanesulfonate&amp;#8211;dichloromethane&amp;#8211;n-hexane (1/1/0.5)

subject

description

[1,2-Bis(diphenylphosphanyl)ethane-κ2P,P′]{2-[(4-nitrobenzoylmethyl)diphenylphosphanyl]phenyl-κ2C,C′}palladium(II) trifluoromethanesulfonate–dichloromethane–n-hexane (1/1/0.5)