6533b838fe1ef96bd12a3b4b

RESEARCH PRODUCT

H-bonding schemes of di- and tri-p-benzamides assessed by a combination of electron diffraction, X-ray powder diffraction and solid-state NMR

Anne BohleGalina MatveevaUte KolbAndreas F. M. KilbingerTobias W. SchleussJ. Van De StreekGunther BrunklausTatiana Gorelik

subject

DiffractionCrystallographyElectron diffractionChemistryGeneral Materials ScienceGeneral ChemistryNuclear magnetic resonance crystallographyCrystal structureSelected area diffractionCondensed Matter PhysicsSingle crystalPowder diffractionElectron backscatter diffraction

description

The crystal structures of di- and tri-p-benzamides are solved by a combination of single crystal, electron and powder X-ray diffraction. Different hydrogen-bonding schemes observed in the two structures are described and classified. The hydrogen-bonding networks are correlated to complementary data obtained from multinuclear solid-state NMR.

https://doi.org/10.1039/b920569a