Synthesis of Both Ionic Species of Ammonium Dithiocarbamate Derived Cholic Acid Moieties

6533b83afe1ef96bd12a6f0c

RESEARCH PRODUCT

Synthesis of Both Ionic Species of Ammonium Dithiocarbamate Derived Cholic Acid Moieties

Erkki Kolehmainen Juha Koivukorpi

subject

Magnetic Resonance Spectroscopy medicine.drug_class Sodium Chemistry Pharmaceutical Pharmaceutical Science chemistry.chemical_element Salt (chemistry)Article Analytical Chemistry Bile Acids and Salts lcsh:QD241-441 chemistry.chemical_compound dithiocarbamate NMR spectroscopy lcsh:Organic chemistry Thiocarbamates Cations Drug Discovery Polymer chemistry parasitic diseases medicine polycyclic compounds Organic chemistry Ammonium Physical and Theoretical Chemistry Dithiocarbamate ta116 chemistry.chemical_classification Ions Drug Carriers Bile acid Organic Chemistry steroid Cholic acid Cationic polymerization Water Cholic Acids Amides cholic acid Quaternary Ammonium Compounds chemistry amine Chemistry (miscellaneous)Carbon Disulfide Molecular Medicine Amine gas treating

description

The reaction of 3-aminopropylamide of cholic acid with CS2 produced a bile acid derivative of dithiocarbamic acid which further formed an ammonium salt with another molecule of 3-aminopropylamide of cholic acid. The cationic 3-ammonium propylamide of cholic acid did not react further with CS2 and the formed salt was stable in the reaction mixture, even when excess CS2 was used. When the reaction was carried out in the presence of aqueous sodium hydroxide, only the bile acid derivative of sodium dithiocarbamate was formed. The dithiocarbamate derivatives were characterized by 1H- and 13C-NMR spectroscopy and ESI-TOF mass spectrometry.

year	journal	country	edition	language
2011-07-01	Molecules

10.3390/molecules16086306 http://www.mdpi.com/1420-3049/16/8/6306/

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