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RESEARCH PRODUCT

Isolation and concentration of organophosphorus pesticides from water using a c18 reversed phase

C.igualada CañasJ.c.moltó CortésG.font PérezJ.mañes Vinuesa

subject

ChromatographyNitrogen–phosphorus detectorElutionChemistryOrganic ChemistryExtraction (chemistry)General MedicinePesticideBiochemistryAnalytical ChemistrySolventchemistry.chemical_compoundVolume (thermodynamics)Gas chromatographyDisulfoton

description

Abstract A simple, rapid and effective method for the extraction and enrichment of organophosphorus pesticides based on the use of Sep-Pak C 18 cartridges was studied as alternative method to those based on extraction with organic solvents. The influence of the elution solvent, pH, salinity and volume of water filtered was studied for ten organophosphorus pesticides. The pesticides were determined by gas chromatography with a BP-1 capillary column and a thermionic detector. Recoveries at the 100 and 200 ng/1 spiking levels were greater than 85%, except for disulfoton.

yearjournalcountryeditionlanguage
1989-01-01Journal of Chromatography A
https://doi.org/10.1016/s0021-9673(00)94135-9