6533b853fe1ef96bd12acb97
RESEARCH PRODUCT
Determination of hexacelsian by infrared spectroscopy.
Guillem Villar M CMonzonís C Gsubject
ChemistryAnalytical chemistryInfrared spectroscopyHexagonal crystalsParticle sizeAnalytical Chemistrydescription
Hexacelsian has been determined by infrared spectroscopy with KBr discs and K(4)Fe(CN)(6) as internal standard. A KBr particle size of40 mum gave better homogenization of the sample-KBr mixture than a particle size in the 40-70 mum range. For determinations of hexacelsian in synthetic samples containing amorphous phase or celsian, calibration curves were constructed. A least-squares fit yielded correlation coefficients of 0.998 and 0.997.
year | journal | country | edition | language |
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1984-07-01 | Talanta |