Synthesis, Structure, and Magnetic Properties of the Oxalate-Based Bimetallic Ferromagnetic Chain {[K(18-crown-6)][Mn(H2O)2Cr(ox)3]}∞ (18-crown-6 = C12H24O6, ox = C2O42-)

6533b855fe1ef96bd12b1ba5

RESEARCH PRODUCT

Synthesis, Structure, and Magnetic Properties of the Oxalate-Based Bimetallic Ferromagnetic Chain {[K(18-crown-6)][Mn(H2O)2Cr(ox)3]}∞ (18-crown-6 = C12H24O6, ox = C2O42-)

Eugenio Coronado Carlos Marti-gastaldo José Ramón Galán-mascarós Carlos J. Gómez-garcía

subject

Inorganic Chemistry Crystallography chemistry.chemical_compound Nuclear magnetic resonance Chain (algebraic topology)Ferromagnetism Hydrogen bond Chemistry 18-Crown-6 Physical and Theoretical Chemistry Bimetallic strip Oxalate Magnetic exchange

description

The salt [K(18-crown-6)][Mn(H2O)2Cr(ox)3]·0.5(18-crown-6) (1) has been prepared and structurally and magnetically characterized. It crystallizes in the P21/c space group [a = 21.011(2) A, b = 11.265(2) A, c = 15.748(3) A, β = 105.952(6)°, V = 3584(1) A3, and Z = 4] and contains [Mn(H2O)2Cr(ox)3]∞ chains connected through hydrogen bonding to form 2D anionic networks. The magnetic exchange is ferromagnetic [J = +2.23(2) cm-1] in the chain and also in between chains, reaching bulk ferromagnetic ordering below 3.5 K.

year	journal	country	edition	language
2005-08-02	Inorganic Chemistry

https://doi.org/10.1021/ic050258w

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