Development and application of mass spectrometric methods for the determination of Maillard reaction products in foodstuffs

6533b858fe1ef96bd12b67be

RESEARCH PRODUCT

Development and application of mass spectrometric methods for the determination of Maillard reaction products in foodstuffs

subject

Chemistry Analītiskā ķīmija Analytical chemistry Ķīmija

description

Tika izstrādātas jaunas analītiskā s metodes divu pārtikas produktos sastopamo toksikantu noteikšanai, kuri rodas produktos Maijāra reakcijas rezultātā. Pirmo reizi zinātniskajā literatūrā Orbitrap masspektr o metra analītiskās spējas tika piemērotas akrilamīda noteikšanai kafijas paraugos. Izstrādātā metode uzrādīja selektīvu un precīzu detektēšan as spēju mazu molekulu, kā akrilamīds, kvantitatīv ai noteikšan ai sarežģītās matricās, piemēram, kafijā. Instruments nodrošina augstu izšķirtspēju, ļoti labu jūtību, lineāru diapazonu un labu atkārtojamību. Izstrādātā s m etodes salīdzinājums ar tandēma kvadrupola detektēšanas metodi uzrādīja pārākumu šim konkrētajam analīzes veidam. Kafijas paraugu analīze atklāja, ka akrilamīda saturs dažiem paraugiem pārsn iedz Eiropas Komisijas uzrādītos ieteikumus. Tvaika fāzes līdzs vara gāz u hromatogrāfija ar tandēma masspektrometru selektīvajā skenēšanas režīmā , analizējot furānu, uzrādīja augstu jūtību un selektivitāti, novēršot traucēj ošos signālus no citiem matricas komponentiem. Š ajā pētījumā ir noteikts furāna saturs bērnu pārtikā un citos Latvijā ražotos pārtikas produktos. Darbā tika izpētītas akrilamīda satura mazināšanas stratēģijas un iespējamie furāna veidošanās prekursori pārtikas produktos.

year	journal	country	edition	language
2016-01-01

https://dspace.lu.lv/dspace/handle/7/31808

PEPhysical Sciences and Engineering
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