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RESEARCH PRODUCT

Solid-Phase Extraction of Organochlorine Pesticides from Water Samples

Guillermina FontJordi MañesJuan Carlos MoltóC. Albelda

subject

ChromatographyPesticide residueChemistryElutionHealth Toxicology and MutagenesisExtraction (chemistry)Public Health Environmental and Occupational HealthSoil SciencePesticidePollutionAnalytical ChemistryElectron capture detectorAdsorptionEnvironmental ChemistrySolid phase extractionGas chromatographyWaste Management and DisposalWater Science and Technology

description

Abstract A procedure for the accumulation of organochiorine pesticides by reversed-phase adsorption on octadecylsilica glass microcolumns was used for the isolation and concentration from spiked distilled and natural waters. The pesticides were eluted from the octadecylsilica with light petroleum, and analyzed by gas chromatography using an electron capture detector. The average recovery was over 90% in spiked water samples at 0.1 ng/ml. The performance of the octadecylsilica when applied to the analysis of water samples were compared with the Rodier and the APHA solvent extraction methods.

https://doi.org/10.1080/03067319008030525